不同烧结周期对全轮廓单片氧化锆抗弯强度影响的体外比较研究

Sanath Kumar Shetty, Feba Maria Varghese, Mohammed Zahid, Kevin Fernandes, Fahad Mohammad, Prakyath Malli
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The purpose of this study was to evaluate and compare the effect of different sintering cycles on the flexural strength of full-contour monolithic zirconia. \nMETHODS \nIn this in-vitro study, a total of 44 bar-shaped zirconia samples (Amann Girrbach Ceramill® CAD/CAM Material – ZOLID HT+) of final dimensions 20 x 4 x 2 mm were fabricated using Amann Girrbach Ceramill mind – computer-aided designing software and Amann Girrbach Ceramill® motion2 – computer-aided milling unit. These samples were randomly allocated into four groups with 11 samples in each group namely, Group 1, 2, 3 and 4 (Group 1: Long sintering cycle, Group 2: Intermediate sintering cycle, Group 3: Short sintering cycle, Group 4: Ultra-short sintering cycle) and sintered under the respective sintering cycles. 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引用次数: 0

摘要

整体氧化锆修复体具有良好的力学性能和美观性。在氧化锆假体的制造过程中,烧结过程是决定最终产品性能的最关键步骤。然而,氧化锆修复的许多问题与烧结循环有关,烧结循环会影响晶体含量和晶粒生长,从而影响其力学性能。本研究的目的是评估和比较不同烧结周期对全轮廓整体氧化锆抗弯强度的影响。方法采用Amann Girrbach Ceramill®CAD/CAM Material - ZOLID HT+,利用Amann Girrbach Ceramill mind -计算机辅助设计软件和Amann Girrbach®motion2 -计算机辅助铣床,制备最终尺寸为20 x 4 x 2 mm的44个条形氧化锆样品(Amann Girrbach Ceramill®CAD/CAM Material - ZOLID HT+)。将样品随机分为4组,每组11个样品,分别为1、2、3、4组(第1组:长烧结周期,第2组:中等烧结周期,第3组:短烧结周期,第4组:超短烧结周期),在各自的烧结周期下烧结。Ceramill®therm (Amann Girrbach)烧结炉提供3个烧结周期,从最长的第1组(19小时)到最短的第3组(8小时),以及中间的第2组(15小时)。锆石(KDS)烧结炉提供了超短的烧结周期族4(2小时)。在万能试验机上采用三点弯曲试验进行抗弯强度试验。采用SPSS软件对收集的数据进行单因素方差分析。结果单因素方差分析显示,四种不同烧结周期下烧结的全轮廓单片氧化锆的抗弯强度差异无统计学意义。(p < 0.05)。结论不同烧结周期对全轮廓整体氧化锆的抗弯强度有一定影响。最长烧结周期(组1)的抗折强度最低,而中间烧结周期(组2)的抗折强度最高。此外,2小时的超短烧结周期(第4组)显示出与其他较长烧结周期组相当的弯曲强度,从而使该周期成为传统烧结周期的可行替代方案,从而使患者“一天一颗牙”成为可能。
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Effect of Different Sintering Cycles on the Flexural Strength of Full Contour Monolithic Zirconia – An In-Vitro Comparative Study
BACKGROUND Monolithic zirconia restorations are known to exhibit good mechanical properties and acceptable aesthetics. During the fabrication of zirconia prostheses, the sintering process is the most critical step which determines the performance of the final product. However, a lot of issues with zirconia restorations were related to sintering cycles which can affect the crystalline content and grain growth that can affect its mechanical properties. The purpose of this study was to evaluate and compare the effect of different sintering cycles on the flexural strength of full-contour monolithic zirconia. METHODS In this in-vitro study, a total of 44 bar-shaped zirconia samples (Amann Girrbach Ceramill® CAD/CAM Material – ZOLID HT+) of final dimensions 20 x 4 x 2 mm were fabricated using Amann Girrbach Ceramill mind – computer-aided designing software and Amann Girrbach Ceramill® motion2 – computer-aided milling unit. These samples were randomly allocated into four groups with 11 samples in each group namely, Group 1, 2, 3 and 4 (Group 1: Long sintering cycle, Group 2: Intermediate sintering cycle, Group 3: Short sintering cycle, Group 4: Ultra-short sintering cycle) and sintered under the respective sintering cycles. The Ceramill® therm (Amann Girrbach) sintering furnace provided 3 sintering cycles ranging from the longest group-1 (19 hours), to the short sintering cycle group-3 (8 hours), with an intermediate sintering cycle group-2 (15 hours). The zircon (KDS) sintering furnace provided an ultra-short sintering cycle group-4 (2 hours). The testing of flexural strength was performed using a three-point bend test on a universal testing machine. Statistical analysis of the collected data was performed by one-way ANOVA using SPSS software. RESULTS One-way ANOVA showed no statistically significant difference in the flexural strength of full-contour monolithic zirconia sintered under the four different sintering cycles. (P > 0.05). CONCLUSIONS The flexural strength of full-contour monolithic zirconia was influenced to some extent by various sintering cycles. The longest sintering cycle (Group 1) showed the least flexural strength whereas the intermediate sintering cycle (Group 2) showed the highest flexural strength. Also, the ultra-short sintering cycle (Group 4) of 2 hours exhibited flexural strength comparable to the rest of the groups with longer sintering cycles, thus making the cycle a viable alternative to the conventional sintering cycles, thereby making the ‘tooth-in-a-day‘ possible for the patients.
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