高能合金化制备微米级硅铝复合粉末过程中的数值模拟:构建可视化和指导制备

IF 1.5 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Micro & Nano Letters Pub Date : 2023-05-24 DOI:10.1049/mna2.12165
Zhen-yu Guo, Xin Zhang, Yan-jun Wang, Si-yuan Zhang, Yin Yin
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引用次数: 0

摘要

硅铝复合粉末是超声速火焰喷涂制备密封胶涂层的重要前驱体。微米级的硅铝复合粉末可以使用行星球磨机制备,但粉末团聚往往会导致复合材料失效。使用相关建模软件建立了球磨机震击器的三维建模,该建模基于离散元法,使用赫兹-明德林接触模型,在指定模拟边界条件后,对球磨机过程进行了模拟和分析。可视化研磨球的频率、尺寸和直径以及球粉重量比等重要工艺参数的影响,系统分析团聚和分散粉末的微观形态和复合条件。结果表明,球磨过程中的球运动主要分为三种具有代表性的类型:球-球碰撞、球对罐壁的挤压运动和球-壁碰撞。当三种运动的比例均匀时,磨球向粉末系统的能量传递效率最高。SEM图像和EDS光谱显示铝粉被充分粉碎,平均粒径低于1μm。铝粉均匀地分布在硅粉的表面上,并且复合硅聚集体的粒度充分减小。
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Numerical simulation using in the preparation process of micron-sized silica–aluminium composite powders by high-energy alloying: Building visualisation and guiding preparation

Silica-aluminium composite powders are important precursors for the preparation of sealant coatings by supersonic flame spraying. Micron-scale silica-aluminium composite powders can be prepared using a planetary ball mill, but powder agglomeration often leads to composite failure. Using relevant modelling software to build the 3D modelling of the ball mill jar, which based on the discrete element method, using the Hertz–Mindlin contact model and after specifying the simulation boundary conditions, the ball mill process was simulated and analysed. Visualise the influence of important process parameters such as frequency, size and diameter of milling balls and ball-to-powder weight ratio, and systematically analyse the microscopic morphology and composite condition of the agglomerated and dispersed powders. The results show that the ball motion during the ball milling process is mainly divided into three representative types: ball–ball impact, ball crushing motion against the jar wall and ball–wall impact. The energy transfer efficiency of the milling balls to the powder system is highest when the ratio of the three types of motion is uniform. SEM images and EDS spectra showed that the aluminium powder was sufficiently crushed, with an average particle size below 1 μm. The aluminium powder was uniformly distributed on the surface of the silicon powder, and the particle size of the composite silicon aggregates was sufficiently reduced.

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来源期刊
Micro & Nano Letters
Micro & Nano Letters 工程技术-材料科学:综合
CiteScore
3.30
自引率
0.00%
发文量
58
审稿时长
2.8 months
期刊介绍: Micro & Nano Letters offers express online publication of short research papers containing the latest advances in miniature and ultraminiature structures and systems. With an average of six weeks to decision, and publication online in advance of each issue, Micro & Nano Letters offers a rapid route for the international dissemination of high quality research findings from both the micro and nano communities. Scope Micro & Nano Letters offers express online publication of short research papers containing the latest advances in micro and nano-scale science, engineering and technology, with at least one dimension ranging from micrometers to nanometers. Micro & Nano Letters offers readers high-quality original research from both the micro and nano communities, and the materials and devices communities. Bridging this gap between materials science and micro and nano-scale devices, Micro & Nano Letters addresses issues in the disciplines of engineering, physical, chemical, and biological science. It places particular emphasis on cross-disciplinary activities and applications. Typical topics include: Micro and nanostructures for the device communities MEMS and NEMS Modelling, simulation and realisation of micro and nanoscale structures, devices and systems, with comparisons to experimental data Synthesis and processing Micro and nano-photonics Molecular machines, circuits and self-assembly Organic and inorganic micro and nanostructures Micro and nano-fluidics
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