利用钝叶单叶藻水提取物生物合成ZnO.Ag2O3:特性和对肝癌细胞的细胞毒性

IF 1.5 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Micro & Nano Letters Pub Date : 2023-06-25 DOI:10.1049/mna2.12170
Majid Halimi Khalil Abad, Mohabat Nadaf, Mohammad Ehsan Taghavizadeh Yazdi
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引用次数: 4

摘要

首次利用钝叶单叶藻的植物提取物制备了氧化锌-氧化银纳米复合材料(ZnO.Ag2O3颗粒)。应用粉末X射线衍射(PXRD)、傅立叶变换光谱(FTIR)、场发射显微镜(FESEM)、能量色散X射线分析(EDX)和透射电子显微镜(TEM)对制备的纳米复合材料的结构、官能团、形态和纯度进行了分析。PXRD揭示了ZnO的组成。颗粒为Ag2O3。对官能团的研究表明,在ZnO的组成中存在一些碳酸杂质以及吸收的水。Ag2O3纳米复合材料。从形态上看,颗粒形成了大小不等的花瓣状。EDX分析还证实了所制备的样品的组成以及在该配方中存在4.78%的银。此外,TEM分析显示,颗粒大小为80.43±46.73 nm的球形和矩形。此外,ZnO。使用Ag2O3颗粒对抗癌症细胞,这表明合成的NC以浓度和时间依赖的方式对癌症肝癌细胞具有毒性作用。
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Biosynthesis of ZnO.Ag2O3 using aqueous extract of Haplophyllum obtusifolium: Characterization and cell toxicity activity against liver carcinoma cells

The zinc oxide-silver oxide nanocomposite (ZnO.Ag2O3 particles) was prepared by using an aqueous plant extract of Haplophyllum obtusifolium for the first time. Powder X-ray diffraction (PXRD), Fourier transforms spectroscopy (FTIR), field emission microscopy (FESEM), energy dispersive X-ray analysis (EDX), and transmission electron microscopy (TEM) were applied to analyze the structure, functional groups, morphology, and purity of the prepared nanocomposite. PXRD revealed the formulation of ZnO.Ag2O3 for the particles. The investigation of functional groups has demonstrated the presence of some carbonated impurities along with absorbed water in the composition of the ZnO.Ag2O3 nanocomposite. Morphologically, particles have formed a petal-like shape with different sizes. The EDX analysis also confirmed the composition of the prepared sample and the presence of 4.78% silver in the formula. Additionally, the TEM analysis revealed spherical and rectangular shapes with a particle size of 80.43 ± 46.73 nm. Moreover, the ZnO.Ag2O3 particles were used against cancer cells, which has shown synthesized NCs have a toxic effect against liver cancer cells in a concentration and time-dependent manner.

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来源期刊
Micro & Nano Letters
Micro & Nano Letters 工程技术-材料科学:综合
CiteScore
3.30
自引率
0.00%
发文量
58
审稿时长
2.8 months
期刊介绍: Micro & Nano Letters offers express online publication of short research papers containing the latest advances in miniature and ultraminiature structures and systems. With an average of six weeks to decision, and publication online in advance of each issue, Micro & Nano Letters offers a rapid route for the international dissemination of high quality research findings from both the micro and nano communities. Scope Micro & Nano Letters offers express online publication of short research papers containing the latest advances in micro and nano-scale science, engineering and technology, with at least one dimension ranging from micrometers to nanometers. Micro & Nano Letters offers readers high-quality original research from both the micro and nano communities, and the materials and devices communities. Bridging this gap between materials science and micro and nano-scale devices, Micro & Nano Letters addresses issues in the disciplines of engineering, physical, chemical, and biological science. It places particular emphasis on cross-disciplinary activities and applications. Typical topics include: Micro and nanostructures for the device communities MEMS and NEMS Modelling, simulation and realisation of micro and nanoscale structures, devices and systems, with comparisons to experimental data Synthesis and processing Micro and nano-photonics Molecular machines, circuits and self-assembly Organic and inorganic micro and nanostructures Micro and nano-fluidics
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