铜/氮化硅复合材料的制备与表征

IF 1.9 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Advances in Materials Research-An International Journal Pub Date : 2016-09-25 DOI:10.12989/AMR.2016.5.3.131
M. A. Ahmed, W. Daoush, A. El-Nikhaily
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引用次数: 5

摘要

。采用粉末工艺制备了铜/氮化硅(Cu/ si3n4)复合材料。铜作为金属基体,非常细的Si 3n4颗粒(小于1微米)作为增强材料。用所研究的粉末制备了不同Si 3 N 4重量百分比(2、4、6、8和10)的均相(Cu/Si 3 N 4)复合混合物。采用不同温度(850、950、1000、1050℃)对制备的Cu/ si3n4复合材料进行冷压和烧结,并采用SEM和XRD分析制备的Cu/ si3n4复合材料的微观结构和化学成分。结果表明,si3n4颗粒均匀分布在Cu基体中。测定了制备的Cu/ si3n4复合材料的密度、电导率和热膨胀系数。增加铜基体中增强相(si3n4)的含量,降低了相对生坯密度、烧结密度、电导率和热膨胀系数。随着烧结温度的升高,Cu/ si3n4复合材料的烧结密度和电导率均有所提高。
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Fabrication and characterization of Copper/Silicon Nitride composites
. Copper/silicon nitride (Cu/Si 3 N 4 ) composites are fabricated by powder technology process. Copper is used as metal matrix and very fine Si 3 N 4 particles (less than 1 micron) as reinforcement material. The investigated powder were used to prepare homogenous (Cu/Si 3 N 4 ) composite mixtures with different Si 3 N 4 weight percentage (2, 4, 6, 8 and10). The produced mixtures were cold pressed and sintered at different temperatures (850, 950, 1000, 1050 ° C). The microstructure and the chemical composition of the produced Cu/Si 3 N 4 composites were investigated by (SEM) and XRD. It was observed that the Si 3 N 4 particles were homogeneously distributed in the Cu matrix. The density, electrical conductivity and coefficient of thermal expansion of the produced Cu/Si 3 N 4 composites were measured. The relative green density, sintered density, electrical conductivity as well as coefficient of thermal expansion were decreased by increasing the reinforcement phase (Si 3 N 4 ) content in the copper matrix. It is also founded that the sintered density and electrical conductivity of the Cu/Si 3 N 4 composites were increased by increase the sintering temperature.
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来源期刊
Advances in Materials Research-An International Journal
Advances in Materials Research-An International Journal MATERIALS SCIENCE, MULTIDISCIPLINARY-
CiteScore
3.50
自引率
27.30%
发文量
0
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