M. R. Quirino, G. L. Lucena, Renata Júlia Cordeiro de Araújo, Adriano Ribeiro da Silva, Anely Maciel de Melo, I. Santos, L. Gama
{"title":"微波湿热法制备CuO及ce掺杂CuO光降解雷马唑金黄色染料","authors":"M. R. Quirino, G. L. Lucena, Renata Júlia Cordeiro de Araújo, Adriano Ribeiro da Silva, Anely Maciel de Melo, I. Santos, L. Gama","doi":"10.1590/1980-5373-mr-2022-0300","DOIUrl":null,"url":null,"abstract":"Copper oxide (CuO) is a heterogeneous catalyst applied with success in several systems like vegetable oils transesterifications. The Ce-dopoing CuO is a promisor material with a potential improve catalysis performances. In this work, CuO and Ce-doping CuO were synthesized by the microwave hydrothermal method in only 5 min at low temperature (100 o C) without templates or other petroleum dependent organic substances, using only copper and cerium nitrates and sodium hydroxide as a precursors. Both materials were applied as photocatalysts for the degradation of remazol golden yellow dye (RNL). X-ray diffraction analysis showed that CuO and Ce-doped CuO has monoclic copper oxide structure without secondary phases. SEM analysis showed the Ce-doping full modify the CuO powder morphology. The dye RNL degradation rate of Ce-doping CuO was bigger than pure CuO and the expensive CeO 2 .","PeriodicalId":18331,"journal":{"name":"Materials Research-ibero-american Journal of Materials","volume":"1 1","pages":""},"PeriodicalIF":1.5000,"publicationDate":"2023-01-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"CuO and Ce-doped CuO Prepared by Microwave Hidrotermal Method in Photodegradation of Remazol Golden Yellow Dye\",\"authors\":\"M. R. Quirino, G. L. Lucena, Renata Júlia Cordeiro de Araújo, Adriano Ribeiro da Silva, Anely Maciel de Melo, I. Santos, L. Gama\",\"doi\":\"10.1590/1980-5373-mr-2022-0300\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Copper oxide (CuO) is a heterogeneous catalyst applied with success in several systems like vegetable oils transesterifications. The Ce-dopoing CuO is a promisor material with a potential improve catalysis performances. In this work, CuO and Ce-doping CuO were synthesized by the microwave hydrothermal method in only 5 min at low temperature (100 o C) without templates or other petroleum dependent organic substances, using only copper and cerium nitrates and sodium hydroxide as a precursors. Both materials were applied as photocatalysts for the degradation of remazol golden yellow dye (RNL). X-ray diffraction analysis showed that CuO and Ce-doped CuO has monoclic copper oxide structure without secondary phases. SEM analysis showed the Ce-doping full modify the CuO powder morphology. The dye RNL degradation rate of Ce-doping CuO was bigger than pure CuO and the expensive CeO 2 .\",\"PeriodicalId\":18331,\"journal\":{\"name\":\"Materials Research-ibero-american Journal of Materials\",\"volume\":\"1 1\",\"pages\":\"\"},\"PeriodicalIF\":1.5000,\"publicationDate\":\"2023-01-06\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Materials Research-ibero-american Journal of Materials\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.1590/1980-5373-mr-2022-0300\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Materials Research-ibero-american Journal of Materials","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.1590/1980-5373-mr-2022-0300","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
CuO and Ce-doped CuO Prepared by Microwave Hidrotermal Method in Photodegradation of Remazol Golden Yellow Dye
Copper oxide (CuO) is a heterogeneous catalyst applied with success in several systems like vegetable oils transesterifications. The Ce-dopoing CuO is a promisor material with a potential improve catalysis performances. In this work, CuO and Ce-doping CuO were synthesized by the microwave hydrothermal method in only 5 min at low temperature (100 o C) without templates or other petroleum dependent organic substances, using only copper and cerium nitrates and sodium hydroxide as a precursors. Both materials were applied as photocatalysts for the degradation of remazol golden yellow dye (RNL). X-ray diffraction analysis showed that CuO and Ce-doped CuO has monoclic copper oxide structure without secondary phases. SEM analysis showed the Ce-doping full modify the CuO powder morphology. The dye RNL degradation rate of Ce-doping CuO was bigger than pure CuO and the expensive CeO 2 .