Fe-Ti-M(M=Al,Si,Co)三元薄膜的结构与软磁性能

N. Aoyama;F. Sato;Y. Fujino;T. Miyazaki
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引用次数: 1

摘要

研究了溅射Fe-Al-Ti、Fe-Si-Ti和Fe-Co-Ti三元薄膜的磁性和结构性能。样品在673K下退火1小时。Fe-Si-Ti和Fe-Co-Ti三元薄膜的晶体结构为bcc,Fe-Al-Ti三三元薄膜为bcc和bcc+Fe2Ti的混合物。Ti的加入减少了&3x001F5;雨的大小最小为约10nm。向Fe中添加Al、Si或Ti降低了Fe-Al-Ti和Fe-Si-Ti膜的饱和磁通密度,而添加Co增加了Fe-Co-Ti的饱和磁通强度。在每个三元体系中都获得了零磁致伸缩样品。Fe-Al-Ti三元薄膜通过添加少量Ti,获得了低矫顽力(5Oe以下)和高初始磁导率(约1000),同时零磁致伸缩。在Fe-Co-Ti三三元薄膜的情况下,获得了小晶粒尺寸(10nm左右)的低矫顽磁力和高磁导率。具有低磁致伸缩性(λs≪3×10-6)的薄膜具有与晶粒直径的三次方大致成比例的矫顽力。
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Structure and Soft Magnetic Properties of Fe-Ti-M (M=Al,Si,Co) Ternary Films
The magnetic and structural properties of sputtered Fe-Al-Ti, Fe-Si-Ti and Fe-Co-Ti ternary films were investigated. Samples were annealed at 673K for one hour. Crystal structures were bcc for the Fe-Si-Ti and Fe-Co-Ti ternary films, and a mixture of bcc and bcc+Fe 2 Ti for the Fe-Al-Ti ternary films. The addition of Ti reduces &3x001F5;rain sizes to a minimum of about 10 nm. Addition of Al, Si or Ti to Fe reduces the saturation magnetic flux density of Fe-Al-Ti and Fe-Si-Ti films, and addition of Co increases the saturation magnetic flux density of Fe-Co-Ti. Zero-magnetostriction samples were obtained in each ternary system. Low coercivity (under 5 Oe) and high initial permeability (about 1000) were obtained together with zero magnetostriction for Fe-Al-Ti ternary films by adding a small amount of Ti. In the case of Fe-Co-Ti ternary films, low coercivity and high permeability were obtained along with small grain sizes of 10 nm or so. Films with low magnetostriction (λ s ≪3×10 -6 ) had a coercivity roughly proportional to the third power of the grain diameter.
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