N. Petrasauskiene, E. Paluckiene, R. Alaburdaitė, M. Gilić
{"title":"聚酰胺表面硫化铜膜的沉积","authors":"N. Petrasauskiene, E. Paluckiene, R. Alaburdaitė, M. Gilić","doi":"10.2298/sos2202139p","DOIUrl":null,"url":null,"abstract":"In this paper, we present a novel and low - cost method for preparing copper sulfide films on polyamide. Non-treated as well as pre-treated PA6 films by 3 different methods (in boiled water; in NaOH solution; in boiled water and then in NaOH solution) were used for the formation of Cu2S layers by the sorption-diffusion method. Molten sulfur has been used as a sulfurization agent. The XRD, FTIR, and UV-VIS methods were used to characterize the structural, optical, and electrical properties of samples and to track changes in samples after each treatment stage. The sheet resistance of Cu2S layers depends on the pre-treatment method and varied from 7 k?/sq to 6 M?/sq. The optical band gaps (Eg) for direct and indirect transitions are determined to be 2.61-2.67 eV and 1.40-1.44 eV, respectively. Furthermore, the optical constants n, k, and ? are determined from UV-VIS measurements.","PeriodicalId":21592,"journal":{"name":"Science of Sintering","volume":"1 1","pages":""},"PeriodicalIF":1.4000,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Deposition of copper sulfide films on polyamide surface\",\"authors\":\"N. Petrasauskiene, E. Paluckiene, R. Alaburdaitė, M. Gilić\",\"doi\":\"10.2298/sos2202139p\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this paper, we present a novel and low - cost method for preparing copper sulfide films on polyamide. Non-treated as well as pre-treated PA6 films by 3 different methods (in boiled water; in NaOH solution; in boiled water and then in NaOH solution) were used for the formation of Cu2S layers by the sorption-diffusion method. Molten sulfur has been used as a sulfurization agent. The XRD, FTIR, and UV-VIS methods were used to characterize the structural, optical, and electrical properties of samples and to track changes in samples after each treatment stage. The sheet resistance of Cu2S layers depends on the pre-treatment method and varied from 7 k?/sq to 6 M?/sq. The optical band gaps (Eg) for direct and indirect transitions are determined to be 2.61-2.67 eV and 1.40-1.44 eV, respectively. Furthermore, the optical constants n, k, and ? are determined from UV-VIS measurements.\",\"PeriodicalId\":21592,\"journal\":{\"name\":\"Science of Sintering\",\"volume\":\"1 1\",\"pages\":\"\"},\"PeriodicalIF\":1.4000,\"publicationDate\":\"2022-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Science of Sintering\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://doi.org/10.2298/sos2202139p\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"MATERIALS SCIENCE, CERAMICS\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Science of Sintering","FirstCategoryId":"88","ListUrlMain":"https://doi.org/10.2298/sos2202139p","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"MATERIALS SCIENCE, CERAMICS","Score":null,"Total":0}
Deposition of copper sulfide films on polyamide surface
In this paper, we present a novel and low - cost method for preparing copper sulfide films on polyamide. Non-treated as well as pre-treated PA6 films by 3 different methods (in boiled water; in NaOH solution; in boiled water and then in NaOH solution) were used for the formation of Cu2S layers by the sorption-diffusion method. Molten sulfur has been used as a sulfurization agent. The XRD, FTIR, and UV-VIS methods were used to characterize the structural, optical, and electrical properties of samples and to track changes in samples after each treatment stage. The sheet resistance of Cu2S layers depends on the pre-treatment method and varied from 7 k?/sq to 6 M?/sq. The optical band gaps (Eg) for direct and indirect transitions are determined to be 2.61-2.67 eV and 1.40-1.44 eV, respectively. Furthermore, the optical constants n, k, and ? are determined from UV-VIS measurements.
期刊介绍:
Science of Sintering is a unique journal in the field of science and technology of sintering.
Science of Sintering publishes papers on all aspects of theoretical and experimental studies, which can contribute to the better understanding of the behavior of powders and similar materials during consolidation processes. Emphasis is laid on those aspects of the science of materials that are concerned with the thermodynamics, kinetics and mechanism of sintering and related processes. In accordance with the significance of disperse materials for the sintering technology, papers dealing with the question of ultradisperse powders, tribochemical activation and catalysis are also published.
Science of Sintering journal is published four times a year.
Types of contribution: Original research papers, Review articles, Letters to Editor, Book reviews.