退火冷拔低碳钢再结晶动力学及组织演变

Nurudeen A. Raji, O. Oluwole
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引用次数: 12

摘要

研究了0.12 wt% C冷拔钢在600℃和650℃退火过程中的再结晶行为。硬度试验用于表征再结晶动力学。利用光学显微镜(OM)对未处理和退火钢试样的晶粒组织进行了表征。在650℃退火后,所有变形钢的位错缺陷均在5 ~ 10分钟内消失。特别是在5分钟的浸泡时间内,晶粒的伸长仍然存在,这表明晶粒没有发生改造,而是变形晶粒的恢复。在退火时间为10分钟时,观察到新的晶粒开始形成,在退火时间为15分钟时实现了完全再结晶。在退火时间为20 ~ 25分钟时,观察到晶粒变粗,表明晶粒开始长大。在各种冷拉变形程度下,材料的硬度随退火温度的升高而降低。根据实验得到的硬度值,退火钢的再结晶随着冷拉变形程度的增加而增加。与55%冷拔钢相比,20%冷拔钢的恢复过程延长。恢复过程的延长是由于驱动力的减少。根据冷拔钢的程度不同,在不同的浸泡时间内,退火钢的完全再结晶得以实现。
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Recrystallization Kinetics and Microstructure Evolution of Annealed Cold-Drawn Low-Carbon Steel
The recrystallization behavior of cold-drawn 0.12 wt% C steel during annealing at temperatures 600˚C and 650˚C was investigated. Hardness tests were used to characterize the recrystallization kinetics. The micrographs of the steel were obtained using optical microscopy (OM) to characterize the grain microstructure of the non-treated and the annealed steel samples. Annihilation of dislocation defects occur within the soaking time of 5 - 10 minutes for all the deformed steel after annealing at 650˚C. Specifically at 5 minutes soaking time the grains elongation is still observed indicating that reformation of grains is not taking place but recovery of the deformed grains. At the 10 minutes annealing time, new grains are observed to begin and full recrystallization is achieved at 15 minutes annealing time. At annealing time between 20 - 25 minutes, grains coarsening are observed indicating the onset of grain growth. The hardness of the material reduces with increasing annealing temperature for all the degree of cold drawn deformation. On the basis of the experimentally obtained hardness values, recrystallization increases with increasing degree of cold drawn deformation for the annealed steel. Recovery process was found to prolong in the 20% cold drawn steel as compared to the 55% cold drawn steel. The prolong recovery process is due to reduction in the driving force. Full recrystallization of the annealed steel is achieved at different soaking time depending on the degree of the cold drawn steel.
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