实验室制造的光反应器的设计、表征和评估:迈向光催化标准化程序的第一步**

IF 6.1 Q1 CHEMISTRY, MULTIDISCIPLINARY Chemistry methods : new approaches to solving problems in chemistry Pub Date : 2023-06-09 DOI:10.1002/cmtd.202300002
Dr. Thomas Aubineau, Dr. Justine Laurent, Ludovic Olanier, Dr. Amandine Guérinot
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引用次数: 0

摘要

在过去的十五年里,随着新的光氧化还原方法的出现,以及新的强大人工光源的开发,光化学已经得到了更新。然而,即使在使用商业设备时,所描述的过程也经常缺乏关于设置的特性(波长、实际接收的光功率、距光源的距离)的信息。这一空白信息阻碍了标准化程序的发展,而标准化程序将保证反应的再现性。为了提供一个标准化的设置,设计了一个实验室制造的反应器。3D打印技术的使用使大多数实验室都能轻松访问它。它的表征表明了环境条件对所接收的光功率的关键影响,以及它们对光化学反应的再现性有多么重要。最后,根据最近文献中的实验对该装置进行了评估。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

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Design, Characterization and Evaluation of a Lab-made Photoreactor: A First Step Towards Standardized Procedures in Photocatalysis**

For the last fifteen years, photochemistry has known a renewal with the emergence of new photoredox approaches, along with the development of new powerful artificial sources of light. However, the described procedures often lack information about the characteristics of the setups (wavelength, actual received light power, distance from the source) even when commercial apparatuses are used. This lacunar information hampers the development of standardized procedures which would guarantee the reproducibility of the reactions. With the objective of furnishing a standardized setup, a lab-made reactor was designed. The use of 3D-printing technology makes it easily accessible to most laboratories. Its characterization showed the critical effect of the environmental conditions upon the light power received and how crucial they are for reproducibility of photochemical reactions. At last, the setup was evaluated against experiments taken from recent literature.

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