溶胶-凝胶法微波合成CaTiO3纳米颗粒

V. F. Kostryukov, A. E. Igonina
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引用次数: 0

摘要

提出了一种微波活化合成纳米钛酸钙粉体的方法。当使用碳酸钠作为沉淀剂时,微波效应用于合成CaTiO3样品,可以获得化学均匀的纳米粉末,并显着减少了工艺时间。References1。张强,Saito F. Fe2O3晶粒尺寸对其与La2O3机械化学反应生成lafeo3的影响。材料科学,2001;36(9):2287-2290。DOI: https://doi.org/10.1023/a: 10175208069222。张建军,李建军,李建军,等。甲烷部分氧化制合成气的制备及其性能研究。欧洲陶瓷学会杂志。27 2007;(6): 2455 - 2461。DOI: https://doi.org/10.1016/j.jeurceramsoc.2006.10.0043。列日尼琴科v.a.,阿维林v.v.,奥列尼娜t.v.。钛酸盐,钛酸盐,钛酸盐。科学基础,技术,生产]。莫斯科:Nauka Publ;2010. 72页(俄文)纳米技术:纳米团簇、纳米结构和纳米材料的物理化学[j]。莫斯科:KomKniga出版。2006. 592页(俄文)古谢夫。纳米材料,纳米结构,纳米技术[j]。莫斯科:Fizmatlit pub .;2007. 416年六年级。国际衍射数据中心。ASTM x射线衍射日期卡
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Microwave Synthesis of CaTiO3 Nanoparticles by the Sol-Gel Method
A technique for the microwave-activated synthesis of calcium titanate nanopowder was proposed. The microwave effect used in the synthesis of CaTiO3 samples when using sodium carbonate as a precipitant allowed obtaining a chemically homogeneous nanopowder with a significant reduction of the process time.       References1. Zhang Q., Saito F. Effect of Fe2O3 crystallite sizeon its mechanochemical reaction with La2O3 to formLaFeO3. Journal of Materials Science. 2001;36(9):2287–2290. DOI: https://doi.org/10.1023/a:10175208069222. Bayraktar D., Clemens F., Diethelm S., et al.Production and properties of substituted LaFeO3‑perovskitetubular membranes for partial oxidation ofmethane to syngas. Journal of the European CeramicSociety. 2007;27(6): 2455–2461. DOI: https://doi.org/10.1016/j.jeurceramsoc.2006.10.0043. Reznichenko V. A., Averin V. V., Olyunina T. V.Titanaty. Nauchnye osnovy, tekhnologiya, proizvodstvo[Titanates. Scientific foundations, technology, production].Moscow: Nauka Publ.; 2010. 72 p. (In Russ.)4. Suzdalev I. P. Nanotekhnologiya: fiziko-khimiyananoklasterov, nanostruktur i nanomaterialov[Nanotechnology: physical chemistry of nanoclusters,nanostructures and nanomaterials]. Moscow:KomKniga Publ.; 2006. 592 p. (In Russ.)5. Gusev A. I. Nanomaterialy, nanostruktury,nanotekhnologii [Nanomaterials, nanostructures,nanotechnology]. Moscow: Fizmatlit Publ.; 2007. 416 p.6. International Center for Diffraction Data.7. X-ray diffraction date cards, ASTM
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