旋转和旋转磁控溅射控制膜厚分布

H. Huang, Li Jiang, Yiyun Yao, Zhong Zhang, Zhanshan Wang, R. Qi
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引用次数: 3

摘要

横向梯度多层准直器是高精度衍射仪的重要组成部分。它被用作冷凝反射器,将来自实验室x射线源的发散x射线转换成平行光束。多层膜的厚度随入射角的变化而变化,以保证反射镜上的每个位置都满足布拉格反射。原则上,溅射条件参数的准确性对于获得可靠的结果至关重要。本文提出了一种基于行星运动磁控溅射控制薄膜厚度的精密制备方法。该方法采用快慢粒子模型获得粒子输运过程,并将其与行星运动磁控溅射系统相结合,建立薄膜厚度分布模型。此外,模型中的溅射条件参数通过实验反演得到,提高了模型的精度。在最终沉积过程中,基底支架的公转和旋转由根据模型计算的速度曲线来实现。x射线反射测试(XRR)的测量结果表明,涂覆在抛物圆柱形Si衬底上的横向梯度多层膜的厚度误差小于1%,证明了优化方法获得精确膜厚分布的有效性。
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Controlling Film Thickness Distribution by Magnetron Sputtering with Rotation and Revolution
The laterally graded multilayer collimator is a vital part of a high-precision diffractometer. It is applied as condensing reflectors to convert divergent X-rays from laboratory X-ray sources into a parallel beam. The thickness of the multilayer film varies with the angle of incidence to guarantee every position on the mirror satisfies the Bragg reflection. In principle, the accuracy of the parameters of the sputtering conditions is essential for achieving a reliable result. In this paper, we proposed a precise method for the fabrication of the laterally graded multilayer based on a planetary motion magnetron sputtering system for film thickness control. This method uses the fast and slow particle model to obtain the particle transport process, and then combines it with the planetary motion magnetron sputtering system to establish the film thickness distribution model. Moreover, the parameters of the sputtering conditions in the model are derived from experimental inversion to improve accuracy. The revolution and rotation of the substrate holder during the final deposition process are achieved by the speed curve calculated according to the model. Measurement results from the X-ray reflection test (XRR) show that the thickness error of the laterally graded multilayer film, coated on a parabolic cylinder Si substrate, is less than 1%, demonstrating the effectiveness of the optimized method for obtaining accurate film thickness distribution.
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