{"title":"青蒿水提物介导的纳米钯生物合成及其对铃木偶联反应的催化评价","authors":"F. Ahmadi, M. Hekmati, M. Yousefi, H. Veisi","doi":"10.26655/AJNANOMAT.2018.6.1","DOIUrl":null,"url":null,"abstract":"A simple and biological method for the fabrication of palladium nanoparticles (Pd NPs) was developed, applying the non-toxic and sustainable natural extract from Artemisia abrotanum as the reducing, stabilizing and capping agent. UV-vis spectroscopy, X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and energy dispersive X-ray spectroscopy (EDS), were utilized to classify the synthesized Pd NPs@Artemisia catalyst. The Pd NPs@Artemisia demonstrated excellent behavior as a reusable nanocatalyst in Suzuki-Miyaura cross-coupling reactions at room temperature. The nanocatalyst was recycled 7 times without any significant deduction in catalytic activity.","PeriodicalId":8523,"journal":{"name":"Asian Journal of Nanoscience and Materials","volume":"14 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2018-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"8","resultStr":"{\"title\":\"Biogenic synthesis of Palladium nanoparticles mediated by Artemisia abrotanum aqueous extract and its catalytic evaluation for Suzuki coupling reactions\",\"authors\":\"F. Ahmadi, M. Hekmati, M. Yousefi, H. Veisi\",\"doi\":\"10.26655/AJNANOMAT.2018.6.1\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A simple and biological method for the fabrication of palladium nanoparticles (Pd NPs) was developed, applying the non-toxic and sustainable natural extract from Artemisia abrotanum as the reducing, stabilizing and capping agent. UV-vis spectroscopy, X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and energy dispersive X-ray spectroscopy (EDS), were utilized to classify the synthesized Pd NPs@Artemisia catalyst. The Pd NPs@Artemisia demonstrated excellent behavior as a reusable nanocatalyst in Suzuki-Miyaura cross-coupling reactions at room temperature. The nanocatalyst was recycled 7 times without any significant deduction in catalytic activity.\",\"PeriodicalId\":8523,\"journal\":{\"name\":\"Asian Journal of Nanoscience and Materials\",\"volume\":\"14 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2018-06-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"8\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Asian Journal of Nanoscience and Materials\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.26655/AJNANOMAT.2018.6.1\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Asian Journal of Nanoscience and Materials","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.26655/AJNANOMAT.2018.6.1","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Biogenic synthesis of Palladium nanoparticles mediated by Artemisia abrotanum aqueous extract and its catalytic evaluation for Suzuki coupling reactions
A simple and biological method for the fabrication of palladium nanoparticles (Pd NPs) was developed, applying the non-toxic and sustainable natural extract from Artemisia abrotanum as the reducing, stabilizing and capping agent. UV-vis spectroscopy, X-ray diffraction (XRD), Fourier transformed infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and energy dispersive X-ray spectroscopy (EDS), were utilized to classify the synthesized Pd NPs@Artemisia catalyst. The Pd NPs@Artemisia demonstrated excellent behavior as a reusable nanocatalyst in Suzuki-Miyaura cross-coupling reactions at room temperature. The nanocatalyst was recycled 7 times without any significant deduction in catalytic activity.