葡萄糖酸钠的合成、表征及其对硅酸盐水泥性能的影响

Mahdee Muhammad Nafee, Umme Sarmeen Akhtar, Md. Sagirul Islam, M. E. Halim, M. G. Mostafa, Imdadul Haque
{"title":"葡萄糖酸钠的合成、表征及其对硅酸盐水泥性能的影响","authors":"Mahdee Muhammad Nafee, Umme Sarmeen Akhtar, Md. Sagirul Islam, M. E. Halim, M. G. Mostafa, Imdadul Haque","doi":"10.9734/irjpac/2023/v24i4817","DOIUrl":null,"url":null,"abstract":"The research explores the synthesis and characterization of sodium gluconate as a retarding admixture for Ordinary Portland Cement (OPC) and its impact on cement properties. The study found that sodium gluconate prolonged OPC's setting time, enhancing workability. Sodium gluconate was synthesized through a simple chemical process involving the reaction of gluconic acid with sodium hydroxide. The synthesized product was characterized using Fourier Transform Infrared (FTIR) and 1H-NMR spectroscopy. The results showed that the synthesized sodium gluconate had a characteristic absorption peak at 3205 cm1.The variations were investigated for setting time, compressive strength, and porosity. However, higher dosages led to prolong the setting time, increased the workability, reduced compressive strength and improved porosity. The study emphasizes the importance of balancing sodium gluconate dosage with other locally available admixtures for desired retardation effects without compromising strength. Further research is needed to optimize dosage and explore long-term effects on cement properties.","PeriodicalId":14371,"journal":{"name":"International Research Journal of Pure and Applied Chemistry","volume":"143 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2023-08-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis and Characterization of Sodium Gluconate and Its Effects on the Properties of Portland Cement\",\"authors\":\"Mahdee Muhammad Nafee, Umme Sarmeen Akhtar, Md. Sagirul Islam, M. E. Halim, M. G. Mostafa, Imdadul Haque\",\"doi\":\"10.9734/irjpac/2023/v24i4817\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The research explores the synthesis and characterization of sodium gluconate as a retarding admixture for Ordinary Portland Cement (OPC) and its impact on cement properties. The study found that sodium gluconate prolonged OPC's setting time, enhancing workability. Sodium gluconate was synthesized through a simple chemical process involving the reaction of gluconic acid with sodium hydroxide. The synthesized product was characterized using Fourier Transform Infrared (FTIR) and 1H-NMR spectroscopy. The results showed that the synthesized sodium gluconate had a characteristic absorption peak at 3205 cm1.The variations were investigated for setting time, compressive strength, and porosity. However, higher dosages led to prolong the setting time, increased the workability, reduced compressive strength and improved porosity. The study emphasizes the importance of balancing sodium gluconate dosage with other locally available admixtures for desired retardation effects without compromising strength. Further research is needed to optimize dosage and explore long-term effects on cement properties.\",\"PeriodicalId\":14371,\"journal\":{\"name\":\"International Research Journal of Pure and Applied Chemistry\",\"volume\":\"143 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-08-09\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Research Journal of Pure and Applied Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.9734/irjpac/2023/v24i4817\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Research Journal of Pure and Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.9734/irjpac/2023/v24i4817","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

研究了普通硅酸盐水泥(OPC)缓凝剂葡萄糖酸钠的合成、表征及其对水泥性能的影响。研究发现,葡萄糖酸钠延长了OPC的凝固时间,提高了和易性。以葡萄糖酸和氢氧化钠为原料,通过简单的化学反应合成了葡萄糖酸钠。利用红外傅立叶变换(FTIR)和核磁共振(1H-NMR)对合成产物进行了表征。结果表明,合成的葡萄糖酸钠在3205 cm2处有一个特征吸收峰。研究了凝固时间、抗压强度和孔隙率的变化。然而,较高的掺量延长了凝固时间,提高了和易性,降低了抗压强度,提高了孔隙率。该研究强调了平衡葡萄糖酸钠剂量与其他当地可用的外加剂的重要性,以获得所需的缓凝效果而不影响强度。需要进一步的研究来优化用量并探索对水泥性能的长期影响。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Synthesis and Characterization of Sodium Gluconate and Its Effects on the Properties of Portland Cement
The research explores the synthesis and characterization of sodium gluconate as a retarding admixture for Ordinary Portland Cement (OPC) and its impact on cement properties. The study found that sodium gluconate prolonged OPC's setting time, enhancing workability. Sodium gluconate was synthesized through a simple chemical process involving the reaction of gluconic acid with sodium hydroxide. The synthesized product was characterized using Fourier Transform Infrared (FTIR) and 1H-NMR spectroscopy. The results showed that the synthesized sodium gluconate had a characteristic absorption peak at 3205 cm1.The variations were investigated for setting time, compressive strength, and porosity. However, higher dosages led to prolong the setting time, increased the workability, reduced compressive strength and improved porosity. The study emphasizes the importance of balancing sodium gluconate dosage with other locally available admixtures for desired retardation effects without compromising strength. Further research is needed to optimize dosage and explore long-term effects on cement properties.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Kinetics and Equilibrium Studies of the Detoxification of Aqueous Solutions of Phenolic Derivatives using Activated Carbon Anti-Diabetic Activities of the Extracts from Euphorbia hirta L. (Euphorbiaceae) Specie found in Burkina Faso Using α-Glucosidase Inhibitor Syntheses and X-ray Structure of N-(Benzothiazol-2-yl)-3-chlorobenzamide Copper Adsorption by a Clay from Central Ivory Coast: Analysis by Differential Pulse Anodic Stripping Voltammetry Isolation and Characterization of Glucocorticoid Steriod from the Leaf of Rauvolfia vomitoria
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1