μ-PD法制备SrB4O7透明晶体光纤

Takaaki Machida, Shouichi Inaba, Maki Ueda, Harutoshi Asakawa, R. Komatsu
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引用次数: 3

摘要

采用微下拉(μ-PD)法生长SrB4O7 (SBO)透明晶体纤维,拉伸速率为0.01 ~ 0.40 mm/min。我们用光学显微镜观察了SBO晶体。在VP为0.40 mm/min时,SBO晶体纤维由于空洞的掺入而浑浊。相比之下,在VP小于0.02 mm/min的情况下,可以获得透明的单晶纤维。这是首次培育出长度达几厘米的透明SBO晶体纤维。这些结果表明,在低VP下生长SBO晶体是获得透明晶体纤维的关键。此外,利用SBO晶体生长速率与孔洞扩散速率之间的关系,考虑了SBO晶体中孔洞的产生机理。
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Growth of transparent SrB4O7 crystal fiber by the μ-PD method
We grew transparent SrB4O7 (SBO) crystal fibers by the micro-pulling-down (μ-PD) method at pulling rates (VP) of 0.01–0.40 mm/min. We observed the SBO crystals by optical microscopy. The SBO crystal fiber at VP of 0.40 mm/min was cloudy due to the incorporation of voids. In contrast, transparent single-crystal fibers were obtained at VP of less than 0.02 mm/min. This is the first time that transparent SBO crystal fibers have been grown with a length of several centimeters. These results demonstrate that it is crucial to grow SBO crystals at a low VP to obtain transparent crystal fibers. In addition, we considered the generation mechanism of voids in the SBO crystals by using the relation between the growth rate of SBO crystals and the diffusion rate of voids.
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