产自加纳的酸水解玉米和木薯淀粉葡萄糖当量分析

Odum Bismark, Owusu Kwaku Michael, Odoom Kwesi Justice, E. Otoo, Norgbey Eyram, Kwakye Danso Benjamin
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引用次数: 0

摘要

用酸水解法将淀粉转化为葡萄糖既困难又耗时。该工艺需要高酸性介质和温度,这往往会污染最终产物水解物。因此,本研究通过改变初始淀粉浓度和酸体积来获得生产高质量葡萄糖当量所需的最佳条件。玉米淀粉和木薯淀粉的质量为100 ~ 400 g,水解用盐酸的总体积为1 ~ 3 l。结果表明,两种淀粉水解为葡萄糖的最佳条件为:温度100℃~ 120℃,淀粉浓度12 w/w%, 4大气压,操作时间30 min。最佳条件下木薯淀粉和玉米淀粉的葡萄糖当量分别为79.80%和78.66%。过程中产生的葡萄糖量是温度、压力、酸量、操作时间和初始淀粉浓度的函数。实验结果还证实,随着温度的升高,水解液的pH值也会增加,这影响了葡萄糖的质量。这些结果提供了新的发现,补充了关于初始淀粉浓度和酸体积如何通过酸型水解影响葡萄糖当量的现有结果。
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Dextrose Equivalent Analysis of Acid Hydrolysed Corn and Cassava Starch Sourced from Ghana
The use of acid hydrolysis to convert starch into dextrose can be difficult and time-consuming. The process requires high acidic medium and temperature which tends to contaminate the end-product hydrolysate. Therefore, this research was carried out to obtain optimum conditions necessary to produce a high and quality Dextrose Equivalent by varying the initial starch concentration and acid volume. The mass of corn and cassava starch and the total hydrochloric acid volume used for the hydrolysis ranged from 100 to 400 g and 1-3 liters respectively. The results showed that the optimum conditions for hydrolyzing the two starch types to Dextrose were within a temperature range of 100°C-120°C, 12 w/w% starch concentration, 4 atmospheric pressure and 30 minutes operating time. The optimum conditions produced a Dextrose Equivalent of 79.80% and 78.66% for cassava and corn starch respectively. The amount of dextrose produced in the process is a function of temperature, pressure, acid volume, operating time and initial starch concentration. Experimental results also confirmed an increase in pH of the hydrolysate with a temperature rise, and this influenced the Dextrose quality. The outcomes provided new findings to complement existing outcomes on how initial starch concentration and acid volume affect Dextrose Equivalent by acid-type hydrolysis.
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