机械(压缩)驱动形式通过位错滑移触发了Ti-5553合金亚稳态β相场中β相向α相转变

T. Ali, L. Wang, Xingwang Cheng, Yangwei Wang, H. Cheng, Binbin Zhang, Anjin Liu, Xuefeng Xu, Zhenlu Zhou, Zixuan Ning, Ziqi Xu, Xinhua Min
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摘要

大多数结构合金的应用是在静态、动态和循环载荷形式下进行的,本文对Ti-5553合金在β相场中的变形和相变机理进行了研究,以确定准静态和动态压缩作用下的变形和相变机理。为了获得完全的β相场,将Ti-5553合金在900℃(比β温度高出近50℃)的温度下加热1小时,然后空气淬火。随后,分别以103/s应变速率和10-3/s应变速率进行Split Hopkinson压杆(SHPB)动态压缩(DC)和准静态压缩(QSC)。利用OM、SEM、HRTEM、EBSD等不同的工具对回收的标本进行了全面的检查,以获得可靠的数据来证明逻辑结论。结果表明,QSC和DC的变形方式均以位错滑移和一定程度的缠绕为主,但前者晶界滑移和剥落更为明显。饱和位错滑移晶粒发生相转变,其中β (BCC)向ω转变是通过机械动力的形式完成的,即两个相邻(110)ᵦ面在(111)ᵦ方向上的剪切量相等但方向相反的两个相邻(111)ᵦ面之间的总分离距离的±1/6,这可以通过两个紧密存在的(110)ᵦ面转变为ω后收缩3%来证明。此外,还注意到在位错滑移饱和的晶粒中发生了ω相和α相变。
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Mechanical (Compressive) Form of Driving Force Triggered the Phase Transformation from Beta to Omega & Alpha Phases by Means of Dislocation Slips in Metastable Beta Phase Field Ti-5553 Alloy
Most of structural alloys' applications are under static, dynamic and cyclic forms of loading, for which Ti-5553 alloy in beta phase field is being investigated to confirm the mechanism of deformation and phase transformation upon quasi-static and dynamic compression. To achieve the fully beta phase field, Ti-5553 alloy was heated at 900oC (almost 50oC above beta tarsus temp.) for one hour of soaking time followed by air quenching. Thereafter, Dynamic compression (DC) by Split Hopkinson Pressure Bar (SHPB) and Quasi-static compression (QSC) were performed at strain rate of 103/s and 10-3/s, respectively. Recovered specimens were thoroughly examined by using different tools such as OM, SEM, HRTEM, EBSD to get reliable data for justification of logical conclusions. It's found that the prominent mode of deformation was dislocation slips along with twining to some extent in both of QSC and DC but sliding and spalling of grain boundary was more noticeable in former. Transformation of phases occurred in saturated dislocation slips grains in which from beta (BCC) to omega transformation has been completed by mechanical form of driving force in a way when set of two adjacent (110)ᵦ planes covered ±1/6 of total separation distance between two next to each other (111)ᵦ planes, equal but opposite shears, in (111)ᵦ direction and it could be justified by the 3% shrinkage of two closely existed (110)ᵦ planes after transformation to omega. Furthermore, it is noticed that the omega phase and alpha transformation occurred in the grains which were saturated with dislocation slips.
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