还原氧化石墨烯上一锅水热合成纳米银增强抗菌和抗氧化性能的表征

R. Rajeswari, H. Prabu, Dr.M. Amutha
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引用次数: 7

摘要

石墨烯基纳米复合材料在催化、电子、医药、能源等领域具有重要的应用价值。本文以硝酸银为前驱体,采用一锅水热法制备了还原氧化石墨烯纳米复合材料银纳米粒子。采用水热法在不使用化学试剂的情况下将氧化石墨烯还原为还原性氧化石墨烯。采用XRD、紫外可见光谱、扫描电镜和拉曼光谱对合成的Ag-RGO纳米复合材料进行了表征。研究了复合材料对革兰氏阳性菌和革兰氏阴性菌的抑菌活性。结果表明,Ag-RGO纳米复合材料对革兰氏阴性菌具有较强的杀菌剂作用。通过DPPH自由基清除实验,对氧化石墨烯、Ag和Ag- rgo纳米复合材料的抗氧化活性进行了评价。结果表明,Ag/RGO纳米复合材料的抗氧化活性明显高于单纯的氧化石墨烯和Ag。
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One Pot Hydrothermal Synthesis Characterizations Of Silver Nanoparticles On Reduced Graphene Oxide For Its Enhanced Antibacterial And Antioxidant Properties.
Graphene-based nanocomposite have significant applicability in catalysis, electronics, medicine, and energy. In this report silver nanoparticles (AgNPs) with Reduced Graphene Oxide (RGO) nanocomposite was prepared by a one-pot hydrothermal process using silver nitrate as a precursor. Under hydrothermal process Graphene oxide (GO) was reduced to reduced graphene oxide (RGO), without using chemical reagents. As synthesized (Ag-RGO) nanocomposite was characterized by XRD, UV Vis-spectroscopy, Scanning electron microscope, and Raman spectroscopy. Antimicrobial activities of the composite were investigated against both Gram-positive and Gram-negative bacteria. The results demonstrate that Ag-RGO nanocomposite was a strong bactericide against Gram-negative bacteria. Antioxidant activity was evaluated for bare GO, Ag and Ag-RGO nanocomposite by DPPH radical scavenging assay. It was observed that Ag/RGO nanocomposite has enhanced antioxidant activity than bare GO and Ag.
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