微陶瓷颗粒增强环氧聚合物的统计分析

Arthur Bernardes Lara Melo, Luís Fernando Lucas Paiva, Júlio Cesar dos Santos, T.H. Panzera, R. Freire
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引用次数: 7

摘要

大量的研究集中在利用陶瓷纳米/微颗粒来提高聚合物基体的强度和刚度上。本研究评估了硅酸盐水泥或结晶二氧化硅(石英)颗粒包裹体对环氧聚合物的影响。在全因子设计分析的基础上进行了两个实验。实验1研究了硅酸盐水泥用量(ASTM III)、两种硬化剂(HY 951和956)以及两种养护时间(7天和28天)对颗粒复合材料压缩性能和密度的影响。实验二考虑28天的养护时间和HY 951硬化剂,通过混合不同质量分数水平来评价石英或水泥颗粒的掺入情况。样品在随机制造过程中制备,并在压缩中进行测试。使用的硬化剂类型对其力学性能有显著影响。在适当的水平集中考虑,这两种颗粒都可以提高复合材料的抗压强度和刚度。
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A Statistical Analysis of Epoxy Polymer Reinforced with Micro Ceramic Particles
A significant amount of research has been focused on the use of ceramic nano/micro particles to enhance the strength and stiffness of polymeric matrices. This work evaluates the effect of Portland cement or crystalline silica (quartz) particle inclusions into epoxy polymer. Two experiments were conducted based on a full factorial design analysis. Experiment I investigated the effect of Portland cement amount (ASTM III), two types of hardeners (HY 951 and 956) and two curing times (7 and 28 days) on the compressive behaviour and density of particulate composites. Experiment II evaluated the incorporation of quartz or cement particles by mixing different mass fraction levels, considering 28 days of curing time and HY 951 hardener. The samples were prepared in a randomized manufacturing process and tested in compression. The mechanical properties were significantly affected by the type of hardener used. Both particles, considered in appropriate level set, can enhance the compressive strength and stiffness of the composites.
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