亚硫酰氯促进n -磺酰基甲脒衍生物的改进合成

Phosphorus Sulfur and Silicon and The Related Elements Pub Date : 2017-03-15 DOI:10.1080/10426507.2017.1284843

Ruzeahong Hudabaierdi, Abudureheman Wusiman, Ayinigeer Mulati

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引用次数: 8

摘要

摘要研究了一种改进的n -磺酰基甲脒衍生物的合成方法，在亚硫酰氯的存在下，以氯仿为溶剂直接缩合各种磺酰胺和甲酰胺。详细的合成研究表明，该方法在温和的条件下以高收率得到了所需的产物。

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Improved synthesis of N-sulfonylformamidine derivatives promoted by thionyl chloride

GRAPHICAL ABSTRACT ABSTRACT An improved synthesis of N-sulfonylformamidine derivatives has been developed involving direct condensation of various sulfonamides and formamides in the presence of thionyl chloride using chloroform as solvent. Detailed synthetic studies indicate that this procedure gives the desired products in high yields under mild conditions.

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Phosphorus Sulfur and Silicon and The Related Elements

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