磁集成织物相吸附萃取(MI-FPSE):一个强大的绿色(er)替代样品制备

Analytica Pub Date : 2022-12-02 DOI:10.3390/analytica3040030
V. Samanidou, A. Kabir
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引用次数: 2

摘要

绿色(er)样品制备技术仍然主导着所有分析方案的预期改进。世界各地的分离科学家不断努力满足绿色分析化学(GAC)的要求。为了顺应这一趋势,微萃取技术不断发展,以弥合绿色分析化学和样品预处理之间的差距。2014年,佛罗里达州迈阿密市佛罗里达国际大学的一个研究小组推出了织物相吸附萃取(FPSE)技术,这在当时被认为是微萃取技术的一个新的里程碑。两年后,同一个研究小组推出了一种优势的创新配置,将搅拌和提取机制结合到一个单一的样品制备装置中,保留了经典FPSE最初提供的所有优点。磁集成织物相吸附萃取(MI-FPSE)作为一种新的、有利的FPSE实现方法最终被引入。该装置显示了通过样品扩散提高萃取动力学的有利作用,从而提高了微萃取装置的萃取效率,并支持了结合工艺的需要,以更好地促进和实施绿色分析化学原理。本文介绍了MI-FPSE的应用,展示了该技术在分析和生物分析样品制备中的重要作用。
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Magnet Integrated Fabric Phase Sorptive Extraction (MI-FPSE): A Powerful Green(er) Alternative for Sample Preparation
Green(er) sample preparation technologies still dominate as the anticipated improvement in all analytical protocols. Separation scientists all over the world continuously strive to comply with the Green Analytical Chemistry (GAC) demands. To follow this trend, microextraction techniques are constantly evolving to bridge the gap between Green Analytical Chemistry and sample pretreatment. A research group from Florida International University, Miami, Florida has introduced fabric phase sorptive extraction (FPSE) in 2014 that was considered as a new milestone in microextraction technologies at that time. Two years later, the same research group introduced an advantageous innovative configuration that combines the stirring and extraction mechanism into a single sample preparation device, keeping all the benefits originally offered by classical FPSE. Magnet integrated fabric phase sorptive extraction (MI-FPSE) was eventually introduced as a new, advantageous implementation of FPSE. This device exhibits the advantageous role of the increase in extraction kinetics through sample diffusion, resulting in improved extraction efficiency of the microextraction device and supports the need for combining processes for better promotion and implementation of the principles of Green Analytical Chemistry. The applications of MI-FPSE are presented herein, showing the essential role that this technique can play in analytical and bioanalytical sample preparation.
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