粉末冶金法制备铜杂化纳米复合材料的热吸附及腐蚀特性研究

V. Senthilkumar, A. Nagadeepan, Melvin Victor De Poures, R. Sasikumar, N. Mukilarasan, M. Aruna, C. Priya, Gopal Kaliyaperumal, Elangomathavan Ramaraj
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摘要

陶瓷结合的新结构为工程材料提供了新的机会,通过固态工艺获得增强的材料特性,以克服传统材料在水生应用中的缺点。在上述应用中,铜基材料具有很高的耐腐蚀性和良好的热性能。本研究的主要目的是通过固态加工(粉末冶金)合成含有不同重量百分比氧化铝和石墨硬陶瓷的铜基杂化纳米复合材料的特性。氧化铝纳米粒子的存在和良好的共混工艺提高了样品的耐腐蚀性,石墨纳米粒子可以限制样品在动电位腐蚀分析中的重量损失。所开发的复合材料的显微维氏硬度通过E384标准的ASTM值69 Hv进行评估,并通过增加氧化铝纳米颗粒的重量百分比来注意。制备的复合材料样品的热重分析表明,实际烧结的传导温度在400℃到750℃之间。测试样品的热重图说明曲线发现在427℃~ 456℃之间存在双步分解。用动电位分析仪评价试样的腐蚀行为,用失重方程计算复合材料的理论失重。
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Thermal Adsorption and Corrosion Characteristic Study of Copper Hybrid Nanocomposite Synthesized by Powder Metallurgy Route
Novel constitutions of ceramic bond the new opportunity of engineering materials via solid-state process attaining enhanced material characteristics to overcome the drawback of conventional materials used in aquatic applications. The copper-based materials have great potential to explore high corrosion resistance and good thermal performance in the above applications. The main objectives of this research are to develop and enhance the characteristics of the copper-based hybrid nanocomposite containing different weight percentages of alumina and graphite hard ceramics synthesized via solid-state processing (powder metallurgy). The presence of alumina nanoparticles with a good blending process has to improve the corrosion resistance, and graphite nanoparticles may limit the weight loss of the sample during potentiodynamic corrosion analysis. The developed composite’s micro Vickers hardness is evaluated by the E384 standard on ASTM value of 69 Hv and is noted by increasing the weight percentages of alumina nanoparticles. The conduction temperature of actual sintering anticipates the thermogravimetric analysis of developed composite samples varied from 400°C to 750°C. The thermogravimetric graph illustration curve of the tested sample found double-step decomposition identified between 427°C and 456°C. The potentiodynamic analyzer is used to evaluate the corrosion behaviour of the sample and the weight loss equation adopted for finding the theoretical weight loss of the composite.
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