{"title":"RDX在熔融DNAN/MNA中的溶解度","authors":"G. Luo, Hui Huang, Shuai Zhang, Pingsheng Wang, Zhongzhan Cai, Yong Zhang","doi":"10.3969/J.ISSN.1006-9941.2012.04.012","DOIUrl":null,"url":null,"abstract":"High performance liquid chromatography (HPLC) was employed to analysis the solubility of RDX in melting DNAN/MNA at the range of 87°C to 95.3°C. The optimal chromatography conditions were as following: mobile phase is methanol/water=6/4 (V/V), and flow rate 1.0 mL·min -1, and wavelength of detector 254 nm, and injection volume 5.0 μL. The influence of particle size, equilibration time and temperature programming on solubility was studied. Under the optimum condition, the curve of the solubility of RDX in DNAN/MNA as a function of temperature was built. Results show that the solubility of RDX increases with increasing of the temperature.","PeriodicalId":35753,"journal":{"name":"Hanneng Cailiao/Chinese Journal of Energetic Materials","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2012-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Solubility of RDX in melting DNAN/MNA\",\"authors\":\"G. Luo, Hui Huang, Shuai Zhang, Pingsheng Wang, Zhongzhan Cai, Yong Zhang\",\"doi\":\"10.3969/J.ISSN.1006-9941.2012.04.012\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"High performance liquid chromatography (HPLC) was employed to analysis the solubility of RDX in melting DNAN/MNA at the range of 87°C to 95.3°C. The optimal chromatography conditions were as following: mobile phase is methanol/water=6/4 (V/V), and flow rate 1.0 mL·min -1, and wavelength of detector 254 nm, and injection volume 5.0 μL. The influence of particle size, equilibration time and temperature programming on solubility was studied. Under the optimum condition, the curve of the solubility of RDX in DNAN/MNA as a function of temperature was built. Results show that the solubility of RDX increases with increasing of the temperature.\",\"PeriodicalId\":35753,\"journal\":{\"name\":\"Hanneng Cailiao/Chinese Journal of Energetic Materials\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2012-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Hanneng Cailiao/Chinese Journal of Energetic Materials\",\"FirstCategoryId\":\"1087\",\"ListUrlMain\":\"https://doi.org/10.3969/J.ISSN.1006-9941.2012.04.012\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Engineering\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Hanneng Cailiao/Chinese Journal of Energetic Materials","FirstCategoryId":"1087","ListUrlMain":"https://doi.org/10.3969/J.ISSN.1006-9941.2012.04.012","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Engineering","Score":null,"Total":0}
High performance liquid chromatography (HPLC) was employed to analysis the solubility of RDX in melting DNAN/MNA at the range of 87°C to 95.3°C. The optimal chromatography conditions were as following: mobile phase is methanol/water=6/4 (V/V), and flow rate 1.0 mL·min -1, and wavelength of detector 254 nm, and injection volume 5.0 μL. The influence of particle size, equilibration time and temperature programming on solubility was studied. Under the optimum condition, the curve of the solubility of RDX in DNAN/MNA as a function of temperature was built. Results show that the solubility of RDX increases with increasing of the temperature.
期刊介绍：
Chinese Journal of Energetic Materials is a vital forum for the exchange of science and technology in energetic materials, and information on - Propellants - Explosives - Pyrotechnics - Ignition, combustion and detonation
京公网安备 11010802042870号
京ICP备2023020795号-1
分享
求助内容：
应助结果提醒方式：
扫码关注我们
