聚(MMA)/有机粘土纳米复合材料的合成、表征及热性能

N. Çankaya
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引用次数: 2

摘要

本研究采用原位聚合的方法研究了聚甲基丙烯酸甲酯(MMA)聚合物/粘土基纳米复合材料的合成、表征和热性能。采用红外光谱(FTIR)、x射线衍射(XRD)和热技术对纳米材料进行表征。XRD和TGA测试结果表明,当聚合物基体中粘土含量分别为3%和5%时,纳米复合材料的形貌发生了剥离。热分析表明,粘土比与纳米材料的热稳定性呈正相关。关键词:聚合物/粘土纳米复合材料,有机粘土,热稳定性,原位聚合,甲基丙烯酸甲酯DOI: 10.7176/CMR/12-3-02出版日期:2020年3月31日
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Synthesis, Characterization and Thermal Properties of Poly(MMA)/Organoclay Nanocomposites
In this study, the synthesis, characterization, and thermal properties of poly(methyl methacrylate) (MMA) polymer/clay based nanocomposites were investigated by in situ polymerization. At the characterizations of nanomaterials FTIR, XRD, and thermal techniques were used. It was determined from XRD and TGA measurements that the morphology of nanocomposites was exfoliated when the clay content in the polymer matrix was kept at 3% and 5%. From thermal analysis, a positive correlation was observed between the clay ratio and thermal stability of nanomaterials. Keywords: Polymer/clay nanocomposite, organoclay, thermal stability, in-situ polymerization, methyl methacrylate. DOI: 10.7176/CMR/12-3-02 Publication date: March 31 st 2020
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