均匀沉淀法合成多尺度团聚体

M. Berrada, F. Gray, T. Kuntzsch, M. Coumil
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引用次数: 0

摘要

在搅拌反应器中均相沉淀可得到硫化锌多尺度团聚体。粒径分布和形貌作为几个操作参数的函数进行了研究:pH、反应物浓度(硫乙酰胺和硫酸锌)、温度和搅拌速率。观察到四种尺寸尺度。搅拌速率和pH分别对最大和最小粒径有影响。硫乙酰胺的浓度对最大尺度有影响。所有的尺度都取决于温度。
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Multi‐Scale Agglomerate Synthesis by Homogeneous Precipitation
Zinc sulfide multiscale aggregates can be obtained by homogeneous precipitation in a stirred reactor. Particle size distributions and morphologies are studied as a function of several operating parameters: pH, concentration in reactants (thioacetamide and zinc sulfate), temperature and stirring rate. Four size scales are observed. Stirring rate and pH have an influence respectively on the largest and the smallest size scale. Concentration in thioacetamide has an effect on the largest scales. All size scales depend on temperature.
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