硅烷化SiO2与聚酯纤维复合材料加入热固化丙烯酸树脂的力学性能比较。

A. Fatihallah
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引用次数: 7

摘要

背景:改善聚甲基丙烯酸甲酯(PMMA)树脂的性能是目前面临的挑战,这可以通过在粉末或单体中添加几种形式和类型的纳米和微颗粒来实现,研究的目的是研究添加SiO2纳米颗粒与聚酯纤维结合后丙烯酸树脂的一些力学性能。材料与方法:本研究包括160个样品,分为四组,研究四项测试:横向抗弯强度、冲击强度、表面硬度和表面粗糙度(n=10)。第一组为对照组(未添加),第二组为添加重量为5%的SiO2纳米颗粒,第三组为添加重量为3%,长度为6mm的聚酯纤维,第四组为添加重量为5%的SiO2纳米颗粒和重量为3%,长度为6mm的聚酯纤维的组合。数据分析采用方差分析表和多重比较事后Tukey检验。结果表明:在PMMA树脂中添加5%硅化SiO2和3%长度为6mm的聚酯纤维,其抗冲击强度和抗弯强度均有明显提高;而抗弯强度和表面硬度检验经方差分析表推理统计分析,各组间差异无统计学意义。各组表面粗糙度比较发现,含硅化SiO2组表面粗糙度最高,而含聚酯纤维组表面粗糙度最低。结论:在本研究的限制范围内,硅烷化SiO2和聚酯纤维组合在显著重量和纤维长度下的掺入导致PMMA树脂的冲击和弯曲强度增强,而对表面硬度和粗糙度性能没有或几乎没有影响。
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Comparison of Some Mechanical Properties of Silanated SiO2 and Polyester Fiber Composite Incorporation into Heat Cured Acrylic Resin.
Background: improving polymethylemethacrylate (PMMA) resin properties is the challenge nowadays, this can be done by adding several forms and types of nano- and micro-particles to the powder or to the monomer , the aims of the study is to investigate some mechanical properties of the acrylic resin after the addition of SiO2 nano-particles in combination with polyester fibers. Materials and Methods: The research includes 160 samples divided into four groups, four tests investigated in the study: Transverse flexural strength, impact strength, surface hardness and surface roughness (n=10). Group I is the control (No addition), group II with the addition of SiO2 5% by wt. nano-particles, group III in which polyester fibers 3% by wt., 6 mm length added and group IV contains a combination of SiO2 5% by wt. nano-particles and polyester fibers 3% by wt., 6 mm length. The data analyzed by ANOVA Table and multiple comparison post hoc Tukey’s tests. Results: Show that a mark increase in the impact and flexural strength when combination of 5% by wt. silanated SiO2 and 3% by wt. and 6 mm length polyester fiber incorporated into PMMA resin; while flexural strength and surface hardness tests show that there was no significant differences among the groups after ANOVA Table inferential statistical analysis application. Surface roughness comparison among the groups revealed that group containing silanated SiO2 only gives the highest rough surface while group containing polyester fiber only shows the lowest value of roughness. Conclusion: Within the limitation of this study, incorporation of silanated SiO2 and polyester fiber combinations in a significant weight and fiber length lead to enhancement in the impact and flexural strength of PMMA resins and with no or little effect on the surface hardness and roughness properties.
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