{"title":"SiC/Si-W-Mo涂层在1873 K下保护C/C复合材料","authors":"Dangshe Hou, Kezhi Li, Hejun Li, Qiangang Fu, Yulei Zhang","doi":"10.1016/S1005-8850(08)60294-7","DOIUrl":null,"url":null,"abstract":"<div><p>In order to prevent carbon/carbon composites from oxidation at 1873 K, an efficient oxidation protective SiC/Si-W-Mo coating was prepared by a two-step pack cementation technique. The microstructures and the phase composition of the as-received multi-coating were examined by scanning electron microscopy (SEM) and X-ray diffraction (XRD). It is seen that the compact multi-coating is composed of α-SiC, Si, and (W<sub><em>x</em></sub>Mo<sub>1–<em>x</em></sub>)Si<sub>2</sub>. Oxidation test shows that, after oxidation at 1873 K in air for 102 h and thermal cycling between 1873 K and room temperature for 10 times, the weight loss of the SiC/Si-W-Mo coated C/C composites is only 0.26%. The invalidation of the multi-coating is attributed to the formation of penetrable cracks in the coating.</p></div>","PeriodicalId":100851,"journal":{"name":"Journal of University of Science and Technology Beijing, Mineral, Metallurgy, Material","volume":"15 6","pages":"Pages 822-826"},"PeriodicalIF":0.0000,"publicationDate":"2008-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/S1005-8850(08)60294-7","citationCount":"2","resultStr":"{\"title\":\"SiC/Si-W-Mo coating for protection of C/C composites at 1873 K\",\"authors\":\"Dangshe Hou, Kezhi Li, Hejun Li, Qiangang Fu, Yulei Zhang\",\"doi\":\"10.1016/S1005-8850(08)60294-7\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>In order to prevent carbon/carbon composites from oxidation at 1873 K, an efficient oxidation protective SiC/Si-W-Mo coating was prepared by a two-step pack cementation technique. The microstructures and the phase composition of the as-received multi-coating were examined by scanning electron microscopy (SEM) and X-ray diffraction (XRD). It is seen that the compact multi-coating is composed of α-SiC, Si, and (W<sub><em>x</em></sub>Mo<sub>1–<em>x</em></sub>)Si<sub>2</sub>. Oxidation test shows that, after oxidation at 1873 K in air for 102 h and thermal cycling between 1873 K and room temperature for 10 times, the weight loss of the SiC/Si-W-Mo coated C/C composites is only 0.26%. The invalidation of the multi-coating is attributed to the formation of penetrable cracks in the coating.</p></div>\",\"PeriodicalId\":100851,\"journal\":{\"name\":\"Journal of University of Science and Technology Beijing, Mineral, Metallurgy, Material\",\"volume\":\"15 6\",\"pages\":\"Pages 822-826\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-12-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/S1005-8850(08)60294-7\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of University of Science and Technology Beijing, Mineral, Metallurgy, Material\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1005885008602947\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of University of Science and Technology Beijing, Mineral, Metallurgy, Material","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1005885008602947","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
SiC/Si-W-Mo coating for protection of C/C composites at 1873 K
In order to prevent carbon/carbon composites from oxidation at 1873 K, an efficient oxidation protective SiC/Si-W-Mo coating was prepared by a two-step pack cementation technique. The microstructures and the phase composition of the as-received multi-coating were examined by scanning electron microscopy (SEM) and X-ray diffraction (XRD). It is seen that the compact multi-coating is composed of α-SiC, Si, and (WxMo1–x)Si2. Oxidation test shows that, after oxidation at 1873 K in air for 102 h and thermal cycling between 1873 K and room temperature for 10 times, the weight loss of the SiC/Si-W-Mo coated C/C composites is only 0.26%. The invalidation of the multi-coating is attributed to the formation of penetrable cracks in the coating.