氨基酸溶液纯度关键指标的实验室分析方法

IF 1.7 0 ENGINEERING, PETROLEUM SOCAR Proceedings Pub Date : 2022-12-30 DOI:10.5510/ogp2022si200755
R. Ahiyarov, R. S. Denisov, R. Solovyev
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引用次数: 0

摘要

目前,硫化物气体的净化主要采用胺类溶液,在操作过程中会受到污染,这带来了许多技术问题。我们选择了一系列表征溶液污染程度的关键指标,包括耐热盐的浓度、氯离子的质量分数、铁和镍的质量分数以及发泡溶液。本文介绍了确定溶液污染程度指标的方法的多种描述和本质。为了进行测试,选择了10个再生的MDEA和MEA解决方案。对于得到的每一个值,计算总误差的极限和该值的允许区间,以确定测量的收敛性和充分性。考虑到MI的特征误差,所有的数值都在允许区间内,表明了使用这些方法的可靠性和方便性。关键词:methylethanolamine;methyldiethanolamine;耐热性的盐;腐蚀;导电性;发泡;清洁;活性炭;离子交换树脂。
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Laboratory methods for the analysis of key indicators of the purity of amino solutions
At present, for the purification of gases from sulfur compounds, amine solutions are mainly used, which become contaminated during operation, which entails a number of technological problems. We have chosen a list of key indicators characterizing the degree of contamination of solutions, which consists of the concentration of thermostable salts, the mass fraction of chlorine ions, the mass fraction of iron and nickel, and foaming solutions. The article presents a multiple description and essence of methods for determining the indicators of the degree of contamination of solutions. For testing, 10 regenerated MDEA and MEA solutions were selected. For each value obtained, the limit of the total error and the allowable interval of the value were calculated to determine the convergence and adequacy of the measurements. All values fall within the allowable interval, taking into account the characteristic error of MI, which indicates the reliability and expediency of using these methods. Keywords: methylethanolamine; methyldiethanolamine; thermostable salts; corrosion; electrical conductivity; foaming; cleaning; activated carbon; ion-exchange resin.
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来源期刊
SOCAR Proceedings
SOCAR Proceedings ENGINEERING, PETROLEUM-
CiteScore
3.00
自引率
82.40%
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0
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