{"title":"聚酰亚胺/二氧化硅-钛酸钡纳米复合材料的制备与表征","authors":"Yang Lin","doi":"10.1002/PC.20372","DOIUrl":null,"url":null,"abstract":"The polyimide/silica-barium titanate nanocomposites have been successfully synthesized by a dispersion polymerization method.The morphology,structure and size of the polyimide / silica-barium titanate nanocomposites were investigated by using FT-IR,XRD and TEM.The results indicated that silica-bariumtitanate nanocomposite surface is covered by a thin-layer polymer,the layer thickness is about 10 nm,and the shape of nanocomposite partials is nearly spherical.The crystal structure of BaTiO3 is stable during preparation of narocomposite particles and the chemical bond forms between the inorganic phases and the polymer matrix.","PeriodicalId":17047,"journal":{"name":"Journal of Shaanxi Normal University","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2008-10-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"8","resultStr":"{\"title\":\"Preparation and characterization of polyimide/silica-barium titanate nanocomposites\",\"authors\":\"Yang Lin\",\"doi\":\"10.1002/PC.20372\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The polyimide/silica-barium titanate nanocomposites have been successfully synthesized by a dispersion polymerization method.The morphology,structure and size of the polyimide / silica-barium titanate nanocomposites were investigated by using FT-IR,XRD and TEM.The results indicated that silica-bariumtitanate nanocomposite surface is covered by a thin-layer polymer,the layer thickness is about 10 nm,and the shape of nanocomposite partials is nearly spherical.The crystal structure of BaTiO3 is stable during preparation of narocomposite particles and the chemical bond forms between the inorganic phases and the polymer matrix.\",\"PeriodicalId\":17047,\"journal\":{\"name\":\"Journal of Shaanxi Normal University\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-10-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"8\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Shaanxi Normal University\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1002/PC.20372\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Shaanxi Normal University","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1002/PC.20372","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Preparation and characterization of polyimide/silica-barium titanate nanocomposites
The polyimide/silica-barium titanate nanocomposites have been successfully synthesized by a dispersion polymerization method.The morphology,structure and size of the polyimide / silica-barium titanate nanocomposites were investigated by using FT-IR,XRD and TEM.The results indicated that silica-bariumtitanate nanocomposite surface is covered by a thin-layer polymer,the layer thickness is about 10 nm,and the shape of nanocomposite partials is nearly spherical.The crystal structure of BaTiO3 is stable during preparation of narocomposite particles and the chemical bond forms between the inorganic phases and the polymer matrix.
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