挤压快速凝固Al-10Mg合金粉末的显微组织研究

T. Sheppard, M. Zaidi, G. H. Tan
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引用次数: 20

摘要

摘要采用光学显微镜、扫描电镜和透射电镜观察了Al-10Mg合金快速凝固粉末的显微组织。描述了一种使单个粉末颗粒具有电子透明的技术。合金粉末然后通过冷压巩固,然后使用大范围的温度补偿应变率热挤压。结果表明,显微组织与工艺参数之间存在一定的相关性。研究还表明,初始粉末结构是一个重要的变量。镁在挤出物中以固溶体形式保留,但在室温下是亚稳态的,经过长时间后会分解。然而,观察到的极细晶粒尺寸(1-3 μm)在300°C下是热稳定的,并且可以利用时效工艺获得可接受的组织。
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Microstructural aspects of extrusion of rapidly solidified Al–10Mg alloy powder
AbstractThe microstructures of rapidly solidified Al–10Mg alloy powders have been observed by optical microscopy, scanning electron microscopy, and transmission electron microscopy. A technique is described which enabled individual powder particles to be made electron transparent. The alloy powders were then consolidated by cold compaction followed by hot extrusion using a wide range of temperature compensated strain rates. The microstructures evolved are reported and it is shown that there is a correlation between the microstructures and the process parameters. It is also shown that the initial powder structure is an important variable. Magnesium is retained in solid solution in the extrudate but is metastable at room temperature leading to decomposition over long periods of time. However, the very fine grain size observed (1–3 μm) is thermally stable up to 300°C and aging processes may be utilized to obtain acceptable structures.
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