绿色制备MgO纳米结构的形态学和光学研究

Nagaraja Sannakki, Bharati Basavaraj, B. Sannakki
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引用次数: 1

摘要

以芦荟叶提取物为燃料,采用低温溶液燃烧法制备了绿色合成的多功能氧化镁纳米颗粒。芦荟叶提取物作为制备氧化镁纳米颗粒的燃料。通过PXRD、SEM、TEM和紫外可见光谱等技术对所得MgO纳米粒子进行了进一步表征。利用扫描电子显微镜(SEM)研究了制备样品的表面形貌。PXRD图证实了产物的立方(岩盐)结构。通过PXRD谱计算得到的颗粒粒径在20 ~ 25 nm之间,采用Debye-Scherrer关系。SEM图像显示形成了各种形状的MgO NPs。由于存在本征缺陷中心,NPs表现出突出的绿色发光。光学带隙为4.46 eV。
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Green Fabrication of MgO Nanostructure for Morphology and Optical Studies
Green synthesis of multifunctional magnesium oxide nanoparticles (NPs) were prepared by low temperature solution combustion route employing Aloe vera leaves extract as a fuel. The Aloe vera leaf extracts acts as a fuel in the preparation of MgO nanoparticles. The obtained MgO NPs were further characterized by various techniques such as PXRD, SEM, TEM and UV-visible spectroscopic studies. The surface morphologies of the prepared samples were studied with the help of scanning electron microscopy (SEM). The PXRD pattern confirmed the cubic (halite) structure of the product. The particle size was calculated by means of PXRD profile and it was found to be in the range of 20-25 nm by using the Debye-Scherrer relation. SEM images indicated the formation of various shaped MgO NPs. The NPs exhibited prominent green emission due to the presence of intrinsic defect centers. Also, the results found that the optical band gap is 4.46 eV.
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