电子用粉末注射成型纳米复合材料散热器(MWCNTs/Cu)的研制

A. Muhsan, F. Ahmad
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引用次数: 5

摘要

采用粉末注射成型技术(PIM)成功制备了体积为2.5 Vol. %的多壁碳纳米管(MWCNTs)增强铜基高性能散热器复合材料。采用z型叶片混合器复合Cu/MWCNTs混合物,使固体在粘结剂中均匀分散。用毛细管流变仪测量了在剪切速率范围内的流动特性,这是在金属注射成型过程中预计会发生的。为避免粘结剂降解,进行了TGA试验。TGA结果表明,混合和注塑等工艺温度应低于170℃。注射成型是在低压下进行的。采用溶剂和热脱粘相结合的方法去除样品中的粘结剂,然后在900℃氩气中进行烧结。结果表明:烧结后的样品各向同性收缩率约为21%,重量损失14%,复合材料的密度降低;
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Development of nanocomposites heat sink (MWCNTs/Cu) using powder injection moulding for electronic applications
A fabrication of high performance heat sink composite material made of copper matrix reinforced by multiwalled carbon nanotubes (MWCNTs) up to 2.5 Vol. % using powder injection molding technique (PIM) has been done successfully. A mixture of Cu/MWCNTs was compounded using a Z-blade mixer for homogenous dispersion of solids in the binder. The flow properties were measured using a capillary rheometer in the shear rate range which expected to occur during metal injection molding. To avoid binder degradation, TGA test was carried out. The TGA results showed that the processing temperature such as mixing and injection molding should be lower than 170°C. The injection molding was carried out at low pressure. A combination of solvent and thermal debinding was used for binder removal from the samples and then the sintering process has taken place in argon gas at 900°C. The results show that the sintered samples experience isotropic shrinkage around 21% with 14% weight loss and the density of the composites was decreased after sintering process.
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