变大气热磁法在黄铁矿热分解中的应用

H.J. Hurst, J.H. Levy, S.St.J. Warne
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引用次数: 12

摘要

热磁法研究了黄铁矿分解过程中形成的磁黄铁矿,Fe(1−x)S,在干燥,无氧的氮气中,3%的氢气在氮气中,1.2%的氧气在氮气中。分解被证明比热重测量所能确定的更为复杂。x射线粉末衍射技术,或淬灭黄铁矿样品的化学分析。热磁法被证明是一种灵敏而有用的技术,可以检测分解产物中的许多磁相。
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The application of variable atmosphere thermomagnetometry to the thermal decomposition of pyrite

Thermomagnetometric studies of pyrrhotites, Fe(1−x)S, formed during the decomposition of pyrite, were made in dry, oxygen-free nitrogen, 3% hydrogen in nitrogen, and 1.2% oxygen in nitrogen. Decomposition was demonstrated to be more complex than could be determined by thermogravimetric measurements. X-ray powder diffraction techniques, or chemical analysis of quenched pyrite samples. Thermomagnetometry was shown to be a sensitive and useful technique, enabling the detection of a number of magnetic phases within the decomposition products.

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