研究了在蒸馏水中脉冲激光烧蚀法制备的CdTe纳米颗粒的光学性质和结构性质

Raad S. Alnaily, Murtadha L. Sheqnab
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引用次数: 0

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文章历史:收稿日期:2018年8月12日接受日期:2018年9月5日在线日期:2019年7月22日本文介绍了一种简单有效的制备高纯度、高浓度碲化镉纳米颗粒的方法。采用调q Nd-YAG激光器(100mj, 1064nm, 10ns, 6Hz)和不同的激光脉冲,在蒸馏水中脉冲激光烧蚀合成了CdTe纳米颗粒。利用紫外可见分光光度计测量了CdTe纳米粒子的吸收光谱,发现纳米粒子的浓度与施加激光脉冲的数量有关。利用原子力显微镜(AFM)图像分析证实了纯CdTe纳米颗粒的形成,结果表明生成的CdTe纳米颗粒在纳米尺度上呈白色平均尺寸的球形。利用x射线衍射分析和扫描电镜对纳米颗粒的结构和形貌进行了研究。最后,利用能量色散x射线能谱(EDX)对制备的样品进行元素分析和化学表征,证实制备的样品纯度高,Cd和Te含量高。戴奥。: http://dx.doi.org/10.31257/2018/JKP/2019/110111
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Study the optical and structure properties of CdTe nanoparticles prepared by pulsing laser ablation in distilled water
Article history: Received: 12 AUG, 2018 Accepted: 5 SEP, 2018 Available Online: 22 JUL, 2019 In this paper, an easy and effective method to preparation of cadmium telluride nanoparticles with high purity and concentration have been presented. CdTe nanoparticles were synthesized by pulsed laser ablation in distilled water using Q-switched Nd-YAG laser at (100 mj, 1064 nm, 10ns, 6Hz) and with various laser pulses. The absorption spectra of the CdTe nanoparticles were measured using the UV-Vis spectrophotometer, and found to be affected by concentration of nanoparticles according to the number of applied laser pulses. Formation of the pure CdTe nanoparticles is confirmed using AFM image analysis whose showed that generated CdTe nanoparticles were a spherical shape whit average size in nanoscale. The structural and morphology properties of these nanoparticles were studied using X-ray diffraction analysis and SEM micrograph. Finally, the energy dispersive X-ray spectroscopy (EDX)was employed for the elemental analysis and chemical characterization of a prepared samples, it confirmed that prepared samples was high purity and presence of Cd and Te with high ratio. DIO.: http://dx.doi.org/10.31257/2018/JKP/2019/110111
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