薄层色谱法分析洋桔叶中总萜类化合物的社会化

Jhon Patar Sinurat, Reh Malem Br Karo, R. Berutu
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引用次数: 0

摘要

当使用Liebermann Burchard, Salkowski和cerric sulfate进行测试时,Saputangan叶子含有萜类化合物,呈红棕色环。将三叶浸渍后,用分离漏斗进行分选,得到总萜类化合物,同时用硫酸铈对滤液进行分选。用甲醇溶解的提取物用正己烷拆分,再按1:1的比例在aquadest和乙酸乙酯之间拆分,得到总萜50 g。用正己烷:丙酮(80:20 v/v)溶剂对总萜进行薄层色谱分析。结果表明,总萜类化合物中有11个萜类化合物。根据对参与社会化的参与者进行的测试结果,据称约98%的参与者了解萜类化合物。
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SOCIALIZATION OF ANALYSIS OF TOTAL TERPENOIDS FROM MANILTOA GRANDIFLORA (A. GRAY) SCHEFF LEAVES USING TLC METHODS
Saputangan leaves  contained terpenoids which appeared reddish brown rings when tested using Liebermann Burchard, Salkowski and cerric sulfate. Saputangan leaves were macerated, then partitioned to obtain total terpenoids using a separatory funnel while checking filtrate partition with cerric sulfate. Extracts dissolved with methanol were partitioned with n-Hexane and then partitioned between aquadest and ethyl acetate in a ratio of 1: 1 to obtain 50 g of total terpenoids. TLC analyses was performed on total terpenoids using n-hexane: acetone (80:20 v/v) solvent. The total terpenoids were proved that terpenoids have 11 terpenoids as red stain based on their Rf. Based on the results of tests conducted on participants involved in socialization, it was stated that around 98% of participants had understood terpenoid compounds.
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