基于田口法的CF/PEEK复合材料成型工艺参数优化

Guangming Dai, L. Zhan, Chenglong Guan, Minghui Huang
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引用次数: 5

摘要

本文采用田口L9(33)测试阵列制备了9组层压板,研究了成型压力、成型温度、保温时间3个工艺参数对单向碳纤维/聚醚酮(CF/PEEK)层压板性能的影响。采用差示扫描量热法选择合理的工艺参数范围。测量了复合材料的横向拉伸强度,并通过扫描电镜分析了复合材料的纤维-基体界面结合行为。结果表明,影响横向拉伸强度的因素依次为成型温度、保温时间、成型压力。CF/PEEK复合材料层合板的最佳成型工艺参数为成型温度400℃、成型压力3 MPa、保温时间30 min。优化结果对热塑性复合材料的推广应用具有重要意义。
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Optimization of molding process parameters for CF/PEEK composites based on Taguchi method
In this article, nine groups of laminates were prepared according to the Taguchi L9(33) test array to study the influence of three process parameters, including molding pressure, molding temperature, and holding time on the performance of unidirectional carbon fiber/polyetheretherketone (CF/PEEK) laminates. A differential scanning calorimetry test was employed to select a reasonable process parameters range. The transverse tensile strength of the laminates was measured, and the fiber–matrix interfacial bonding behavior of the tested samples was analyzed by scanning electron microscopy. The results showed that the significance of factors to transverse tensile strength were molding temperature, holding time, and molding pressure in sequence. The optimal molding process parameters for CF/PEEK composite laminate were molding temperature of 400°C, molding pressure of 3 MPa, and holding time of 30 min. The optimization results were meaningful for the extension and application of thermoplastic composites.
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