竹叶提取物制备锌、铜单金属和双金属纳米粒子的绿色合成、表征及生物活性研究

Q2 Chemistry Current Chemistry Letters Pub Date : 2023-01-01 DOI:10.5267/j.ccl.2023.4.002
S. Dubey, A. Shukla, R. Shukla
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引用次数: 0

摘要

本文以牛膝叶提取物为原料,合成了锌、铜单金属和双金属纳米粒子。植物提取物具有表面活性剂和还原剂的双重作用。采用UV-Vis、XRD、FESEM、EDX、HRTEM等技术对合成的纳米颗粒进行了表征。紫外可见光谱用于监测纳米颗粒的合成。采用XRD技术证实了纳米颗粒的无定形性质。FESEM图像表明,纳米粒子的形状为Zn单金属(拟球形)、Cu单金属(棒状)、Zn-Cu双金属(拟球形和棒状)。HRTEM图像显示,Zn、Cu单金属和Zn-Cu双金属纳米颗粒的尺寸分别为3.0 nm、3.52 nm和2.2 nm。EDX光谱证实样品中存在Zn、Cu和O。用合成的锌、铜单金属纳米粒子和锌-铜双金属纳米粒子对其抗菌、抗糖尿病和抗氧化性能进行了评价。与单金属纳米颗粒相比,双金属纳米颗粒显示出更高的抗氧化、抗糖尿病和抗菌性能。结果表明,锌铜双金属纳米粒子比单金属纳米粒子具有更大的潜力。
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Green synthesis, characterization, and biological activities of Zn, Cu monometallic and bimetallic nanoparticles using Borassus flabellifer leaves extract
In the present work, Zn, Cu monometallic and bimetallic nanoparticles were synthesized using leaves extract of Borassus flabellifer. Plant extract acts as both surfactant and reducing agent. The synthesized nanoparticles were characterised by UV-Vis, XRD, FESEM, EDX, and HRTEM techniques. UV-Vis spectroscopy is used to monitor the synthesis of nanoparticles. XRD technique was used to confirm the amorphous nature of nanoparticles. The FESEM images demonstrate that the shape of the nanoparticles such as Zn monometallic (pseudo-spherical), Cu monometallic (rod), Zn-Cu bimetallic are (pseudo-spherical and rod-shaped). HRTEM images show the approximate size of the Zn, Cu monometallic and Zn-Cu bimetallic nanoparticles is 3.0 nm, 3.52 nm and 2.2 nm respectively. EDX spectra confirm the presence of Zn, Cu and O in the sample. Synthesized Zn, Cu monometallic nanoparticles, and Zn-Cu bimetallic nanoparticles were used to evaluate their possible antimicrobial, antidiabetic and antioxidant properties. Bimetallic nanoparticles displayed higher antioxidant, antidiabetic, and antimicrobial properties in the comparison of monometallic nanoparticles. The results suggest that Zn-Cu bimetallic nanoparticles have greater potential than monometallic nanoparticles.
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来源期刊
Current Chemistry Letters
Current Chemistry Letters Chemistry-Chemistry (all)
CiteScore
4.90
自引率
0.00%
发文量
27
审稿时长
20 weeks
期刊介绍: The "Current Chemistry Letters" is a peer-reviewed international journal which aims to publish all the current and outstanding research articles, reviews and letters in chemistry including analytical chemistry, green chemistry, inorganic chemistry, organic chemistry, physical chemistry, etc. This journal is dedicated to serve all academic and industrial researchers and scientists who are expert in all major advances in chemistry research. The journal aims to provide the most complete and reliable source of information on current developments in these fields. The emphasis will be on publishing quality articles rapidly and openly available to researchers worldwide. Please note readers are free to read, download, copy, distribute, print, search, or link to the full texts of articles published on this journal. Current Chemistry Letters is an open access journal, which provides instant access to the full text of research papers without any need for a subscription to the journal where the papers are published. Therefore, anyone has the opportunity to copy, use, redistribute, transmit/display the work publicly and to distribute derivative works, in any sort of digital form for any responsible purpose, subject to appropriate attribution of authorship. Authors who publish their articles may also maintain the copyright of their articles.
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