时效Al-1.0质量%Mg2Si合金中析出相体积分数的定量分析

Katsuya Matsumoto, S. Komatsu, M. Ikeda, B. Verlinden, P. Ratchev
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引用次数: 27

摘要

Al-1.0质量% mg2si合金在473 K时效36ks。对同一试样进行了电阻率(p)测量、拉伸试验和透射电镜观察。根据老化引起的电阻率下降,估算了析出相的体积分数(V fρ)。用TEM显微图测量了单位体积针状析出物的长度(λ)、直径(d)和数量密度(Np)。可能是由于当前时效条件下的过时效引发,λ和Np在独立热处理和测试的两个等效样品中表现出广泛的分散和显著的差异。然而,在两次运行中,证明应力和V fρ相互吻合良好,并且从TEM显微图(V fTEM)估计的体积分数在2倍内匹配。
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Quantification of volume fraction of precipitates in an aged Al-1.0 mass%Mg2Si alloy
An Al-1.0 mass%Mg 2 Si alloy was aged at 473 K for 36ks. Using the same sample, resistivity (p) measurements, tensile tests and TEM observations were carried out. The volume fraction (V fρ ) of precipitates was estimated from the decrement in resistivity due to aging. Length (λ), diameter (d) and number density (Np) per unit volume of the needle-shaped precipitates were measured on TEM micrographs. Perhaps because of initiation of overaging in the present aging condition, λ and Np showed a wide scatter and differed significantly in two equivalent samples, independently heat treated and tested. However, proof stress and V fρ in the two runs well coincided with each other and the volume fraction estimated from TEM micrographs (V fTEM ) matched within a factor of 2 for the two runs.
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