氧化镁和氯化镁纳米颗粒的植物合成优化

H. Shittu, E. Igiehon, A. Eremwanarue, R. E. Oijagbe, M. O. Momoh, M. A. Agbontian
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引用次数: 0

摘要

在本研究中,植物合成了氧化镁(MgO)和氯化镁(MgCl)纳米颗粒。通过对辣木、扁桃叶和竹叶提取物、反应时间、不同浓度氧化镁和氯化镁前体盐、植物提取物与前体盐体积比、介质pH和光源等参数的优化,优化了纳米颗粒的制备效果。采用紫外可见光谱技术对植物合成的氧化镁和氯化镁纳米颗粒进行了表征。研究表明,辣木叶提取物和苦杏仁叶提取物的纳米颗粒含量较高;24小时的孵育时间足以形成纳米颗粒,0.1和0.01摩尔浓度的前驱体盐是纳米颗粒的最佳产率。比例为2(2)的植物提取物与比例为3(3)的前体盐溶液的产率较高;9和11的碱性pH有利于纳米颗粒的合成,可见光源和暗室环境是纳米颗粒形成的较好暴露条件。关键词:叶提取物,氯化镁纳米颗粒,氧化镁纳米颗粒,植物合成,紫外可见光谱
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Optimization of Phytosynthesis of Magnesium Oxide and Magnesium Chloride Nanoparticles
In the present study, magnesium oxide (MgO) and magnesium chloride (MgCl) nanoparticles were phytosynthesized. Selected parameters like leaf extracts from Moringa oleifera, Vernonia amygadalina and Occimum gratissimum, time of reaction, precursor salts of magnesium oxide and magnesium chloride at varying concentrations, plant extracts to precursor salts volume ratio, pH of the medium and light sources were optimized for a better production of the nanoparticles. The phytosynthesized MgO and MgCl nanoparticles were characterized using UV- Vis spectroscopy technique. The study revealed that the leaf extracts of Moringa oleifera and Vernonia amyg dalina yielded more nanoparticles; the period of 24 hours incubation was enough time for nanoparticles formation and the 0.1 and 0.01 molar concentrations of the precursor salts gave optimal yields of the nanoparticles. The plant extracts at ratio two (2) to precursor salt solution at ratio three (3) resulted in better yield of the nanoparticles; the alkaline pH of 9 and 11 gave better nanoparticles synthesis and the visible light source and dark room environments were better exposure conditions for the nanoparticles formation. Keywords: Leaf extracts, Magnesium chloride nanoparticles, Magnesium oxide nanoparticles, Phytosynthesis, UV- Vis spectroscopy.
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