基于电导率的竹中钾的简单定量评价方法

K. Higashi, S. Kawakami, Juri Nakashima, M. Fujisaki, M. Nishioka
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摘要

建立了一种简便的测定竹中钾含量的定量分析方法。以德岛县安安市毛竹为研究对象。在测定钾的方法中,测定了竹材在纯水中灰化和溶解后的电导率。竹材的最佳灰化时间为8 h,因为水溶性磷和交换性磷对竹材电导率的影响在灰化>8 h后消失,且竹材的电导率不变。采用电感耦合等离子体发射光谱法测定了不同竹材样品的电导率和钾含量,并进行了比较。结果显示两者之间有显著的相关性(p <0。1, r2 =0。988)。结果表明,该方法具有良好的标定曲线。因此,所提出的方法可以在不使用昂贵的分析仪的情况下用于现场水平的钾的简单分析。
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Electrical-conductivity-based Simple Quantitative Evaluation Method for Potassium in Bamboo
A simple quantitative analysis method for the detection of potassium in bamboo has been developed. Phyllostachys edulis from Anan City in Tokushima Prefecture was used in this study. In this method of potassium determination, the electrical conductivity of bamboo was measured after ashing and dissolution in pure water. The optimum bamboo ashing time was determined to be 8 h because the effect of water-soluble or exchangeable phosphorus on the electrical conductivity disappeared after bamboo ashing for >8 h and the obtained electrical conductivity was constant. The electrical conductivity and potassium content of various bamboo samples were determined by ICP (Inductively Coupled Plasma) emission spectroscopy and compared. The results showed a significant correlation between them ( p <0 . 01 , r 2 =0 . 988 ). Moreover, the results indicated that a good calibration curve was obtained for this method. Therefore, the proposed method can be used for the simple analysis of potassium at the field level without the use of expensive analyzers.
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