{"title":"非水共沉淀法制备AFe2O4 (A = Mn, Fe, Co, Ni, Zn)基纳米颗粒及其性能","authors":"O. Yelenich, S. Solopan, A. Tovstolytkin","doi":"10.1109/OMEE.2012.6464795","DOIUrl":null,"url":null,"abstract":"In this research crystalline ultrafine nanoparticles of AFe2O4 (A = Mn, Fe, Co, Ni, Zn) compounds with spinel structure have been synthesized by the coprecipitation from nonaqueous solutions method. As the nonaqueous medium was used diethylene glycol. The AFe2O4 nanoparticles were characterized using X-Ray diffraction analysis, thermogravimetric analysis, differential thermal analysis, infrared spectroscopy, vibrating sample magnetometry.","PeriodicalId":6332,"journal":{"name":"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)","volume":"56 1","pages":"71-72"},"PeriodicalIF":0.0000,"publicationDate":"2012-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis and Properties of AFe2O4 (A = Mn, Fe, Co, Ni, Zn)-based nanoparticles coprecipitated from nonaqueous solutions\",\"authors\":\"O. Yelenich, S. Solopan, A. Tovstolytkin\",\"doi\":\"10.1109/OMEE.2012.6464795\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this research crystalline ultrafine nanoparticles of AFe2O4 (A = Mn, Fe, Co, Ni, Zn) compounds with spinel structure have been synthesized by the coprecipitation from nonaqueous solutions method. As the nonaqueous medium was used diethylene glycol. The AFe2O4 nanoparticles were characterized using X-Ray diffraction analysis, thermogravimetric analysis, differential thermal analysis, infrared spectroscopy, vibrating sample magnetometry.\",\"PeriodicalId\":6332,\"journal\":{\"name\":\"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)\",\"volume\":\"56 1\",\"pages\":\"71-72\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2012-09-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/OMEE.2012.6464795\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"2012 IEEE International Conference on Oxide Materials for Electronic Engineering (OMEE)","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/OMEE.2012.6464795","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
本文采用非水溶液共沉淀法合成了具有尖晶石结构的AFe2O4 (A = Mn, Fe, Co, Ni, Zn)晶体超细纳米颗粒。采用二甘醇作为非水介质。采用x射线衍射分析、热重分析、差热分析、红外光谱分析、振动样品磁强分析等方法对纳米AFe2O4进行了表征。
Synthesis and Properties of AFe2O4 (A = Mn, Fe, Co, Ni, Zn)-based nanoparticles coprecipitated from nonaqueous solutions
In this research crystalline ultrafine nanoparticles of AFe2O4 (A = Mn, Fe, Co, Ni, Zn) compounds with spinel structure have been synthesized by the coprecipitation from nonaqueous solutions method. As the nonaqueous medium was used diethylene glycol. The AFe2O4 nanoparticles were characterized using X-Ray diffraction analysis, thermogravimetric analysis, differential thermal analysis, infrared spectroscopy, vibrating sample magnetometry.
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