提取方法对ababa茎α-纤维素性质的影响

S. W. Saragih, B. Wirjosentono, Eddyanto, Y. Meliana
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引用次数: 1

摘要

从abaca茎中提取α-纤维素,采用三种不同的方法提取α-纤维素,然后进行漂白处理。本研究的目的是研究提取方法对abaca茎中α-纤维素性质的影响。第一种方法是不加热的碱化,第二种方法是在80℃温度下辅助加热的碱化,第三种方法是在80℃温度下酸水解和碱化相结合的方法。采用FT-IR、SEM和XRD对所制得的α-纤维素进行了表征。FT-IR光谱分析表明,第三种方法制备的α-纤维素能分离木质素和半纤维素。SEM分析表明,第三种方法得到的α-纤维素表面光滑。第一至第三种方法α-纤维素的结晶度分别为43%、65%和79%。
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The influence of extraction method to the properties of α-cellulose from abaca stem (Musa textillis)
α-cellulose was extracted from abaca stem, where the extraction process was performed using three different methods that followed by bleaching process. The objective of this research was to discover the influence of extraction method to the properties of α-cellulose from abaca stem (Musa textilis). The first method was the alkalization without heating process, the second method was alkalization that assisted with heating process at temperature of 80°C, and the third method was a combination between acid hydrolysis and alkalization at temperature of 80°C. The obtained α-cellulose was characterized using FT-IR, SEM, and XRD. The FT-IR spectra showed the α-cellulose that prepared using third method can separated lignin and hemicellulose from abaca fiber. SEM analysis showed the third method gave the smooth surface of α-cellulose. The crystallinity of α-cellulose was 43, 65, and 79% for first until third method.
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