加热压缩后水溶性组分质量对蒸汽处理竹粉流动性的影响

S. Kajikawa, T. Iizuka
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引用次数: 5

摘要

本研究考察了水溶性组分对蒸汽处理竹粉热流动性的影响。竹粉在180°C或200°C下进行不同时间的蒸汽处理。然后用热水处理竹粉,提取水溶性成分。用毛细管流变仪测定了经热水处理和未处理的经蒸汽处理的竹粉的流速。此外,还采用热重法(TG)考察了热水浸提竹粉的热特性差异。实验结果表明,热水浸提液的量随蒸汽处理温度和时间的变化而变化。流动试验表明,未经热水处理的竹粉具有流动性,而经热水处理的竹粉则不具有流动性。在180℃蒸汽处理下,随着蒸汽处理时间的增加,未处理粉末的流动性能和流速变得稳定和高。在200℃蒸汽处理时,流动行为更稳定,短时间蒸汽处理的流量最高。粉末的热重测定表明,水溶性成分中含有较多的挥发性成分,挥发性成分的含量随着水溶性成分的变性而变化。结果表明,水蒸气处理竹粉的热流动性不仅受水溶性组分含量的影响,还受水溶性组分变性程度的影响。
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Effect of Water-soluble Components Mass on the Fluidity of the Steam-treated Bamboo Powder Caused by Heating and Compression
In this study, the effect of water-soluble components on the thermal fluidity of steam-treated bamboo powder was investigated. Bamboo powders were steam-treated at 180 or 200 °C for various steam treatment times. The bamboo powders were then treated with hot water to extract the water-soluble components. The flow rates of steam-treated bamboo powders that were either treated with hot water or not treated were measured using a capillary rheometer. In addition, thermogravimetry (TG) was also used to examine the differences in the thermal characteristics of bamboo powder treated by hot water extraction. The experimental results indicated that the quantity of hot water extract varied with the steam treatment temperature and time. Flow tests showed that bamboo powders not treated with hot water flowed, whereas those treated with hot water did not flow. The flow behavior and flow rate of the untreated powder became stable and high with an increase in the steam treatment time for steam treatment at 180 °C. For steam treatment at 200 °C, the flow behavior was more stable, and the flow rate became the highest by short time steam treatment. TG measurement of the powders suggested that water-soluble contains many volatile components, and the amount of volatile components changed along with the denaturation of the water soluble components. From these results, it was confirmed that not only the quantity of the water-soluble components but also denaturation of the water soluble component affects the thermal fluidity of the steam-treated bamboo powder.
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