{"title":"电化学沉积法制备ZnO纳米结构的研究与表征","authors":"C.F. Mah, F.K. Yam, Z. Hassan","doi":"10.1016/j.proche.2016.03.119","DOIUrl":null,"url":null,"abstract":"<div><p>ZnO with cube-like nanostructures have been fabricated on tin-doped indium oxide (ITO) coated glass substrates via electrochemical deposition method. The electrolytes used containing equimolar of zinc chloride (ZnCl<sub>2</sub>) and potassium chloride (KCl) ranging from 0.05<!--> <!-->M to 0.2<!--> <!-->M. The samples produced subsequently were examined by field emission scanning electron microscope (FESEM), x-ray diffractometer (XRD), energy dispersive X-ray (EDX) spectroscopy and current transient profile. The average size of the cube-like nano ZnO materials, as observed from FESEM images is decreased from 207<!--> <!-->nm to 102<!--> <!-->nm with increasing of electrolytes concentration. The XRD measurement indicated that the as-deposited nanostructures are converted from amorphous to hexagonal wurtzite ZnO phase after heat treatment at 600<!--> <!-->°C for 3<!--> <!-->hours. Photoresponse measurement revealed that the grown sample is sensitive to the 372<!--> <!-->nm ultraviolet (UV) light.</p></div>","PeriodicalId":20431,"journal":{"name":"Procedia Chemistry","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2016-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/j.proche.2016.03.119","citationCount":"13","resultStr":"{\"title\":\"Investigation and Characterization of ZnO Nanostructures Synthesized by Electrochemical Deposition\",\"authors\":\"C.F. Mah, F.K. Yam, Z. Hassan\",\"doi\":\"10.1016/j.proche.2016.03.119\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>ZnO with cube-like nanostructures have been fabricated on tin-doped indium oxide (ITO) coated glass substrates via electrochemical deposition method. The electrolytes used containing equimolar of zinc chloride (ZnCl<sub>2</sub>) and potassium chloride (KCl) ranging from 0.05<!--> <!-->M to 0.2<!--> <!-->M. The samples produced subsequently were examined by field emission scanning electron microscope (FESEM), x-ray diffractometer (XRD), energy dispersive X-ray (EDX) spectroscopy and current transient profile. The average size of the cube-like nano ZnO materials, as observed from FESEM images is decreased from 207<!--> <!-->nm to 102<!--> <!-->nm with increasing of electrolytes concentration. The XRD measurement indicated that the as-deposited nanostructures are converted from amorphous to hexagonal wurtzite ZnO phase after heat treatment at 600<!--> <!-->°C for 3<!--> <!-->hours. Photoresponse measurement revealed that the grown sample is sensitive to the 372<!--> <!-->nm ultraviolet (UV) light.</p></div>\",\"PeriodicalId\":20431,\"journal\":{\"name\":\"Procedia Chemistry\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2016-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"https://sci-hub-pdf.com/10.1016/j.proche.2016.03.119\",\"citationCount\":\"13\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Procedia Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S1876619616001650\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Procedia Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S1876619616001650","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Investigation and Characterization of ZnO Nanostructures Synthesized by Electrochemical Deposition
ZnO with cube-like nanostructures have been fabricated on tin-doped indium oxide (ITO) coated glass substrates via electrochemical deposition method. The electrolytes used containing equimolar of zinc chloride (ZnCl2) and potassium chloride (KCl) ranging from 0.05 M to 0.2 M. The samples produced subsequently were examined by field emission scanning electron microscope (FESEM), x-ray diffractometer (XRD), energy dispersive X-ray (EDX) spectroscopy and current transient profile. The average size of the cube-like nano ZnO materials, as observed from FESEM images is decreased from 207 nm to 102 nm with increasing of electrolytes concentration. The XRD measurement indicated that the as-deposited nanostructures are converted from amorphous to hexagonal wurtzite ZnO phase after heat treatment at 600 °C for 3 hours. Photoresponse measurement revealed that the grown sample is sensitive to the 372 nm ultraviolet (UV) light.
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