气相色谱-质谱法分析水馏索内奇精油

Mwaura J. Njuguna
{"title":"气相色谱-质谱法分析水馏索内奇精油","authors":"Mwaura J. Njuguna","doi":"10.37284/ijpac.1.1.841","DOIUrl":null,"url":null,"abstract":"The leaves of Solanecio manii were collected from sampled plants in Kandara Sub-County Muranga County in Kenya. The aim of collection of the leaves was to carry out the extraction and analysis of essential oils from S. manii. The leaves were transported to the pharmacognosy laboratory at the Mount Kenya University. The leaves were washed with running tap water and rinsed with distilled water to remove physical and chemical contaminants. They were air dried on the laboratory benches for seven days to lose 90% of moisture content. The essential oils (Eos) were extracted from 200.000 g of dry leaves by hydrodistillation using the Clavenger apparatus for 8 hours. The rate of essential oil production from the leaves was computed and found to be 0.01%. GC-MS instrument was utilized to analyse the qualitative and quantitative composition of essential oils. The compounds that were found present in the total ion chromatogram were, 3-Carene (40%), Limonene (35.48%), 1-undecanol (8.0%), β-pinene (6.4%), Menthol (1.6%), β-Cymene (1.1%) Longifolene (0.78%) and α-terpenolene (0.5%).","PeriodicalId":14371,"journal":{"name":"International Research Journal of Pure and Applied Chemistry","volume":"77 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-09-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Gas Chromatography-Mass Spectrometry Analysis of Hydrodistilled Essentials Oils from Solanecio manii\",\"authors\":\"Mwaura J. Njuguna\",\"doi\":\"10.37284/ijpac.1.1.841\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The leaves of Solanecio manii were collected from sampled plants in Kandara Sub-County Muranga County in Kenya. The aim of collection of the leaves was to carry out the extraction and analysis of essential oils from S. manii. The leaves were transported to the pharmacognosy laboratory at the Mount Kenya University. The leaves were washed with running tap water and rinsed with distilled water to remove physical and chemical contaminants. They were air dried on the laboratory benches for seven days to lose 90% of moisture content. The essential oils (Eos) were extracted from 200.000 g of dry leaves by hydrodistillation using the Clavenger apparatus for 8 hours. The rate of essential oil production from the leaves was computed and found to be 0.01%. GC-MS instrument was utilized to analyse the qualitative and quantitative composition of essential oils. The compounds that were found present in the total ion chromatogram were, 3-Carene (40%), Limonene (35.48%), 1-undecanol (8.0%), β-pinene (6.4%), Menthol (1.6%), β-Cymene (1.1%) Longifolene (0.78%) and α-terpenolene (0.5%).\",\"PeriodicalId\":14371,\"journal\":{\"name\":\"International Research Journal of Pure and Applied Chemistry\",\"volume\":\"77 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-09-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Research Journal of Pure and Applied Chemistry\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.37284/ijpac.1.1.841\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Research Journal of Pure and Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.37284/ijpac.1.1.841","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1

摘要

从肯尼亚穆兰加县坎达拉副县的植物样本中采集了索内奇奥·马尼的叶子。收集叶的目的是提取和分析马尾草的精油。这些叶子被运送到肯尼亚山大学的生药学实验室。用自来水冲洗叶子,用蒸馏水冲洗以去除物理和化学污染物。它们在实验室的工作台上风干7天,以失去90%的水分含量。从200.000 g干叶中提取精油(Eos),用Clavenger装置加氢蒸馏8小时。经计算,其精油提取率为0.01%。采用气相色谱-质谱联用仪对精油成分进行定性和定量分析。总离子图谱中发现的化合物有:3-蒈烯(40%)、柠檬烯(35.48%)、1-十一醇(8.0%)、β-蒎烯(6.4%)、薄荷醇(1.6%)、β-花仙花烯(1.1%)、长叶烯(0.78%)和α-萜烯(0.5%)。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Gas Chromatography-Mass Spectrometry Analysis of Hydrodistilled Essentials Oils from Solanecio manii
The leaves of Solanecio manii were collected from sampled plants in Kandara Sub-County Muranga County in Kenya. The aim of collection of the leaves was to carry out the extraction and analysis of essential oils from S. manii. The leaves were transported to the pharmacognosy laboratory at the Mount Kenya University. The leaves were washed with running tap water and rinsed with distilled water to remove physical and chemical contaminants. They were air dried on the laboratory benches for seven days to lose 90% of moisture content. The essential oils (Eos) were extracted from 200.000 g of dry leaves by hydrodistillation using the Clavenger apparatus for 8 hours. The rate of essential oil production from the leaves was computed and found to be 0.01%. GC-MS instrument was utilized to analyse the qualitative and quantitative composition of essential oils. The compounds that were found present in the total ion chromatogram were, 3-Carene (40%), Limonene (35.48%), 1-undecanol (8.0%), β-pinene (6.4%), Menthol (1.6%), β-Cymene (1.1%) Longifolene (0.78%) and α-terpenolene (0.5%).
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Kinetics and Equilibrium Studies of the Detoxification of Aqueous Solutions of Phenolic Derivatives using Activated Carbon Anti-Diabetic Activities of the Extracts from Euphorbia hirta L. (Euphorbiaceae) Specie found in Burkina Faso Using α-Glucosidase Inhibitor Syntheses and X-ray Structure of N-(Benzothiazol-2-yl)-3-chlorobenzamide Copper Adsorption by a Clay from Central Ivory Coast: Analysis by Differential Pulse Anodic Stripping Voltammetry Isolation and Characterization of Glucocorticoid Steriod from the Leaf of Rauvolfia vomitoria
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1