EN-GJL-250层状灰铸铁的表征及渗硼动力学

IF 0.6 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Annales De Chimie-science Des Materiaux Pub Date : 2020-03-15 DOI:10.18280/acsm.440103
Chaima Zouzou, M. Keddam, B. Bouarour, A. Piasecki, A. Miklaszewski, M. Kulka
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引用次数: 5

摘要

本研究的目的是在层状灰铸铁(EN-GJL-250)表面生成硼化物涂层。在50% B4C、49.5% Al2O3和0.5% AlF3的混合粉末中,分别在800、900和1000℃下进行4、6和8 h的包渗硬化。采用扫描电镜(SEM)和XRD分析对所制备的渗硼层进行表征。对EN-GJL-250片层灰铸铁的渗硼动力学进行了研究。根据实验数据,采用积分扩散模型计算出EN-GJL250铸铁的硼扩散活化能为163.86 kJ mol-1。采用基于实验设计的回归模型(DOE),预测了渗硼工艺参数(渗硼时间和渗硼温度)对渗硼层总厚度的影响。总硼化物层厚度的实验值与回归模型的结果吻合较好。
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Characterization and Boronizing Kinetics of EN-GJL-250 Lamellar Gray Cast Iron
Received: 18 August 2019 Accepted: 5 November 2019 The aim of the present study is to generate the boride coatings at the surface of the lamellar gray cast iron (EN-GJL-250). This material was hardened by pack-boriding in the powders mixture of 50% B4C, 49.5% Al2O3 and 0.5% AlF3 at 800, 900 and 1000°C for 4, 6 and 8 h. The produced borided layers were characterized by Scanning electron microscopy (SEM) and XRD analysis. The boriding kinetics of EN-GJL-250 lamellar gray cast iron was also investigated. Based on the experimental data, the value of activation energy for boron diffusion was calculated as 163.86 kJ mol-1 for the EN-GJL250 cast iron by using the integral diffusion model. The regression model based on the design of experiments (DOE) was also employed in order to predict the total boride layer thickness as a function of boriding parameters (the treatment time and the boriding temperature). The experimental values of total boride layer thickness were in agreement with the results from the regression model.
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来源期刊
Annales De Chimie-science Des Materiaux
Annales De Chimie-science Des Materiaux 工程技术-材料科学:综合
CiteScore
1.70
自引率
25.00%
发文量
33
审稿时长
>12 weeks
期刊介绍: The ACSM is concerning the cutting-edge innovations in solid material science. The journal covers a broad spectrum of scientific fields, ranging all the way from metallurgy, semiconductors, solid mineral compounds, organic macromolecular compounds to composite materials. The editorial board encourages the submission of original papers that deal with all aspects of material science, including but not limited to synthesis and processing, property characterization, reactivity and reaction kinetics, evolution in service, and recycling. The papers should provide new insights into solid materials and make a significant original contribution to knowledge.
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