芒果叶介导的银纳米粒子作为检测抗坏血酸的高效电化学传感器

S. Mamuru, O. O. Joseph, Moorey B. Dalen, Iliya Kaigamma, A. E. Eseyin
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引用次数: 1

摘要

以芒果叶提取物为还原剂,成功地进行了纳米银的生物合成。常用的显微和光谱技术,如紫外-可见。利用FTIR、XRD、EDX、SEM等表征表征了纳米颗粒的形成。经紫外可见光谱证实,银纳米粒子吸收波长约为425 nm的光。光学性质表明,加入植物提取物后,颜色由无色的硝酸银溶液变为黄褐色。傅里叶红外光谱证实了可能导致硝酸银溶液还原的生物分子属于酰胺和酯基团。利用循环伏安法对Pt/AgNP电极进行抗坏血酸氧化的研究表明,银纳米颗粒可以作为抗坏血酸检测的生物传感器。
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Mangifera indica Mediated Synthesis of Silver Nanoparticles as An Efficient Electrochemical Sensor for The Detection of Ascorbic Acid
The biosynthesis of silver nanoparticles using Mangifera indica leaf extract as reducing agent was successfully carried out. The usual microscopic and spectroscopic techniques such as UV-vis., FTIR, XRD, EDX, and SEM were used to confirm the formation of nanoparticles. The silver nanoparticles absorb light at wavelength of approximately 425 nm as confirmed by UV- visible spectroscopy. Optical property showed a colour change from colourless solution of silver nitrate to yellowish brown after addition of the plant extract. The FTIR confirmed the possible biomolecule responsible for the reduction of the silver nitrate solution as belonging to the amide and ester group. Interrogation of Pt/AgNP electrode for ascorbic acid oxidation using cyclic voltammetry suggests that the silver nanoparticles can be a promising candidate as biosensor for ascorbic acid detection.
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