光催化用银修饰TiO2纳米粒子的合成与表征

K. Balachandran, G. Vijayakumar, S. Mageswari, A. Preethi, M.S. Viswak Senan
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引用次数: 1

摘要

以四异丙醇钛为TiO2, AgNO3为Ag前驱体,采用溶胶-凝胶法制备了TiO2纳米粒子(TiO2)和Ag掺杂TiO2纳米复合材料(Ag-TiO2)。采用XRD、SEM、TEM、FT-IR和UV -可见分析对合成的纳米复合材料进行了表征。XRD结果表明,Ag的掺杂使晶粒尺寸由22 nm增大到36 nm。在紫外可见光谱上观察到吸光度的红移,表明晶粒尺寸增大,带隙减小。TEM分析表明,所制备的颗粒均在纳米级范围内。合成的纳米颗粒具有良好的光催化活性,在5小时内就能分解甲基橙染料。
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Synthesis and Characterization of Ag-Decorated TiO2 Nanoparticles for Photocatalytic Application
TiO2 nanoparticles (TiO2) and Ag-doped TiO2 nanocomposites (Ag-TiO2) were synthesized by the Sol-Gel process using titanium tetra isopropoxide as TiO2 and AgNO3 as Ag precursors, respectively. The synthesized nanocomposites were characterized by XRD, SEM, TEM, FT-IR, and UV­-Visible analysis. The XRD results show that Ag doping increases the grain size from 22 nm to 36 nm. From the UV-Visible spectra, the redshift in absorbance was observed, which indicates the increase in grain size and it reduces the bandgap. The TEM analysis shows that all the particles are exhibited in the nanometer range. The synthesized nanoparticles show good photocatalytic activity, and they decompose the methyl orange dye within 5 hours.
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来源期刊
Journal of Water and Environmental Nanotechnology
Journal of Water and Environmental Nanotechnology Materials Science-Materials Science (miscellaneous)
CiteScore
2.40
自引率
0.00%
发文量
0
审稿时长
8 weeks
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