高介孔活性炭吸附水溶液中双氯芬酸的研究

N. Youssef, Ebtsam S. Hamza, S. Shaban
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引用次数: 0

摘要

以含蔗糖的生物质为原料合成介孔碳(MC),以共晶盐(KCl/NaCl)为致孔剂制备蔗糖介孔碳(S-MC)。通过热分析(TGA)、红外光谱(FTIR)、透射电子显微镜(TEM)、x射线衍射(XRD)和BET测量等不同技术对所得样品进行了检测。采用紫外可见光谱法研究了高介孔碳对双氯芬酸的吸附效率。采用紫外可见光谱法测定了不同条件(pH、接触时间、温度、吸附质质量、吸附剂质量)下双氯芬酸的终浓度。关键字;双氯芬酸,蔗糖,介孔碳,紫外光谱。
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Adsorption of Diclofenac from Aqueous Solution Using Highly Meso porous Carbon
Synthetics of mesoporous carbon (MC) from biomass including sucrose was used as the carbon resource, and eutectic salt (KCl/NaCl) as the porogen agent for the preparation of S-MC (sucrose mesopores carbons). The resultant samples were examined by means of different techniques, including thermal analysis (TGA), FTIR, transmitted electron microscopy (TEM), X-ray diffraction (XRD) and BET measurements. Investigate the efficiency of adsorption of diclofenac by highly mesopores carbons using Ultraviolet–Visible spectroscopy. The final concentrations of diclofenac were measured using Ultraviolet–Visible spectroscopy at different conditions (pH, contact time, temperature, weight of adsorbate, weight of adsorbent). Key words; diclofenac, sucrose, meso porous carbon, UV–spectroscopy.
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