锰岩浸出结果制备二氧化锰-石墨烯复合材料及电性能测试

Asri Saleh
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引用次数: 0

摘要

本研究旨在合成并测试锰岩浸出的二氧化锰-石墨烯复合材料的电学性能。测试方法是通过测试电性能的参数,即电容(C),电流(I),电压(V),电阻(R)和电导来完成的。每个测试三种浓度变化,0.25:0.75,0.5:0.05和0.75:0.5。辅助测试参数采用x射线衍射(XRD)和傅里叶变换红外(FTIR)。结果表明,在0.25 gr: 0.75的变化范围内,mno2 -石墨烯复合材料的质量比对电容值的影响为192.3ꙡF,这意味着石墨烯碳比浓度越高,其存储电荷和电能的吸收能力越高。对于353 mV在0.25 gr: 0.75变化时得到的电压变化,在0.25 gr: 0.75变化时得到的电流测试变化值为13.6 mA,在0.25 gr: 0.75变化时得到的电阻值最低为1.6 kΩ。x射线衍射(XRD)测试得到α锰和石墨烯含量为6.8% ~ 93.2%。傅里叶变换红外(FTIR)测试产生Mn-O, CO和OH键。Mn-O的波数分别为479.44 cm-1、1.618.35 cm-1、1.877.47 cm-1和992.07 cm-1。CO波数分别为1104.27 cm-1、1190.69 cm-1和1384.21 cm-1。OH具有波数1438.44 cm-1和1627.70 cm-1的电存储介质。
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Testing of Electrical Properties and Synthesis of MnO2-Graphene Composites from Leaching Results of Manganese Rocks
This study aims to synthesize and test the electrical properties of the MnO2-graphene composite from the leaching of manganese rock. The test method is carried out by testing the electrical properties with the parameters, namely capacitance (C), current (I), voltage (V), resistance (R), and conductometer. Each tested three concentration variations, 0.25: 0.75, 0.5: 0.05, and 0.75: 0.5. Supporting parameters for testing use X-Ray Diffraction (XRD) and Fourier Transform Infrared (FTIR). The results showed that the effect of varying the mass ratio of the MnO2-Graphene composite on the capacitance value was 192.3ꙡF in the variation of 0.25 gr: 0.75, meaning that the higher the concentration of the graphene carbon ratio, the higher the absorption capacity to store charge and electrical energy. For the variation of the voltage obtained by 353 mV at 0.25 gr: 0.75 variations, the current testing variation obtained a value of 13.6 mA at 0.25 gr: 0.75 variations, the variation on resistance obtained the lowest resistance value of 1.6 kΩ in the 0.25 gr variation: 0.75. The X-Ray Diffraction (XRD) test produces α manganese and graphene ranging from 6.8% to 93.2%. The Fourier Transform Infrared (FTIR) test produces Mn-O, CO, and OH bonds. Mn-O with wave numbers 479.44 cm-1, 1.618.35 cm-1, 1.877.47 cm-1, and 992.07 cm-1. CO with wave numbers 1104.27 cm-1, 1190.69 cm-1, and 1384.21 cm-1. OH with wave numbers 1438.44 cm-1 and 1627.70 cm-1 electrical storage medium.
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