反式3-环己基氨基-4-甲氧基-γ-丁内酯的合成、表征和晶体结构

Zhao-Lian Yu, Yuhan Fu, Jian-ge Wang, Sen‐Lan Li
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引用次数: 0

摘要

合成了标题化合物,并通过元素分析、IR、1H NMR、13C NMR等光谱数据和x射线衍射分析对其进行了表征。该化合物在Pbca空间群中以正交晶类结晶。最后的剩余因子R1是0.0510。该分子具有反式立体化学和两个手性中心,因此是外消旋混合物。
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Synthesis, Characterization, and Crystal Structure of trans-3-Cyclohexylamino-4-methoxy-γ-butyrolactone
The title compound was synthesized and characterized by elemental analysis, spectroscopic data such as IR, 1H NMR, 13C NMR, and X-ray diffraction analysis. The compound crystallizes in the orthorhombic crystal class in the space group Pbca. The final residual factor, R1, is 0.0510. The molecule has trans-stereochemistry and two chiral centers, and thus represents a racemic mixture.
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